Fmoc-Asn-[(CH₂)3-NH-Alloc]Tyr-OH

Base Information

Chemical Name:Fmoc-Asn-[(CH₂)3-NH-Alloc]Tyr-OH
CAS No.:1246222-93-4
Molecular Formula:C₃₅H₃₈N₄O₉
Molecular Weight:658.708
Hs Code.:

Fmoc-Asn-[(CH<sub>2</sub>)3-NH-Alloc]Tyr-OH

Synonyms:Fmoc-Asn-[(CH₂)3-NH-Alloc]Tyr-OH

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Fmoc-Asn-[(CH₂)3-NH-Alloc]Tyr-OH

Chemical Property:

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Technology Process of Fmoc-Asn-[(CH₂)3-NH-Alloc]Tyr-OH

There total 4 articles about Fmoc-Asn-[(CH₂)3-NH-Alloc]Tyr-OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 227624-26-2
Alloc-NH-(CH₂)2-CO-N(CH₃)-OCH₃

: 1246222-93-4
Fmoc-Asn-[(CH₂)3-NH-Alloc]Tyr-OH

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

1.2: Saturated solution

2.1: sodium cyanoborohydride; acetic acid / N,N-dimethyl-formamide / solid phase reaction

2.2: 4 h / solid phase reaction

2.3: solid phase reaction

3.1: trifluoroacetic acid / dichloromethane / 2 h

With lithium aluminium tetrahydride; sodium cyanoborohydride; acetic acid; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/psc.1256

Reference yield:

: 1246222-91-2
C₄₅H₅₆N₄O₉

: 1246222-93-4
Fmoc-Asn-[(CH₂)3-NH-Alloc]Tyr-OH

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 2h;
DOI:10.1002/psc.1256

Reference yield:

: 111695-91-1
N-(allyloxycarbonyl)-3-aminopropionic acid

: 1246222-93-4
Fmoc-Asn-[(CH₂)3-NH-Alloc]Tyr-OH

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2.2: Saturated solution

3.1: sodium cyanoborohydride; acetic acid / N,N-dimethyl-formamide / solid phase reaction

3.2: 4 h / solid phase reaction

3.3: solid phase reaction

4.1: trifluoroacetic acid / dichloromethane / 2 h

With lithium aluminium tetrahydride; sodium cyanoborohydride; acetic acid; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/psc.1256