C₂₆H₂₃NO₄S

Base Information

Chemical Name:C₂₆H₂₃NO₄S
CAS No.:1075176-29-2
Molecular Formula:C₂₆H₂₃NO₄S
Molecular Weight:445.539
Hs Code.:

C<sub>26</sub>H<sub>23</sub>NO<sub>4</sub>S

Synonyms:C₂₆H₂₃NO₄S

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Chemical Property of C₂₆H₂₃NO₄S

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Technology Process of C₂₆H₂₃NO₄S

There total 6 articles about C₂₆H₂₃NO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1075176-27-0
C₂₆H₂₃NO₂S

: 1075176-29-2
C₂₆H₂₃NO₄S

Guidance literature:: With ammonium heptamolybdate; dihydrogen peroxide; In ethanol; water; at 0 - 20 ℃; for 16.5h;

Reference yield:

: 632-46-2
2,6-dimethylbenzoic acid

: 1075176-29-2
C₂₆H₂₃NO₄S

Guidance literature:: Multi-step reaction with 7 steps

1.1: borane-THF / tetrahydrofuran / 64.3 h / 0 - 20 °C

2.1: methanol / 48 h / 20 °C

3.1: n-butyllithium / tetrahydrofuran; hexanes / 0.5 h / -78 - 20 °C

3.2: 1 h / -78 - 20 °C

4.1: triethylamine / 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1-methyl-pyrrolidin-2-one / 0.5 h

4.2: 26 h / 80 °C

5.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 0.17 h / 0 °C

6.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0.5 h / 0 °C

7.1: ammonium heptamolybdate; dihydrogen peroxide / ethanol; water / 16.5 h / 0 - 20 °C

With ammonium heptamolybdate; lithium aluminium tetrahydride; n-butyllithium; borane-THF; di-isopropyl azodicarboxylate; dihydrogen peroxide; triethylamine; triphenylphosphine; 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; hexanes; diethyl ether; ethanol; water;

Reference yield:

: 1075176-03-2
(E)-2-(3-iodostyryl)-1,3-dimethylbenzene

: 1075176-29-2
C₂₆H₂₃NO₄S

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1-methyl-pyrrolidin-2-one / 0.5 h

1.2: 26 h / 80 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 0.17 h / 0 °C

3.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0.5 h / 0 °C

4.1: ammonium heptamolybdate; dihydrogen peroxide / ethanol; water / 16.5 h / 0 - 20 °C

With ammonium heptamolybdate; lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; dihydrogen peroxide; triethylamine; triphenylphosphine; 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; diethyl ether; ethanol; water;