C₃₀H₃₄N₂O₇

Base Information

Chemical Name:C₃₀H₃₄N₂O₇
CAS No.:945383-14-2
Molecular Formula:C₃₀H₃₄N₂O₇
Molecular Weight:534.609
Hs Code.:

C<sub>30</sub>H<sub>34</sub>N<sub>2</sub>O<sub>7</sub>

Synonyms:C₃₀H₃₄N₂O₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₀H₃₄N₂O₇

Chemical Property:

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Technology Process of C₃₀H₃₄N₂O₇

There total 12 articles about C₃₀H₃₄N₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₇H₃₂O₇

: 65-71-4,28806-14-6,691841-57-3
thymin

: 945383-14-2
C₃₀H₃₄N₂O₇

Guidance literature:: C₂₇H₃₂O₇; thymin; With N,O-bis-(trimethylsilyl)-acetamide; In acetonitrile; for 0.75h; Heating;

With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 0 - 20 ℃; Further stages.;
DOI:10.1021/ja071106y

Reference yield:

: 945383-12-0
3,5-di-O-benzyl-4-C-penten-yl-1,2-O-isopropylidene-α-D-ribofuranose

: 945383-14-2
C₃₀H₃₄N₂O₇

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid; triflic acid / 0.5 h / ice bath

2.1: N,O-bis(trimethylsilyl)acetamide / acetonitrile / 0.75 h / Heating

2.2: TMSOTf / acetonitrile / 0 - 20 °C

With N,O-bis-(trimethylsilyl)-acetamide; trifluorormethanesulfonic acid; acetic acid; In acetonitrile; 2.2: Vorbrueggen reaction;
DOI:10.1021/ja071106y

Reference yield:

: 945383-09-5
3,5-di-O-benzyl-4-C-hydroxypropyl-1,2-O-isopropylidene-α-D-ribofuranose

: 945383-14-2
C₃₀H₃₄N₂O₇

Guidance literature:: Multi-step reaction with 4 steps

1.1: oxalyl chloride; DMSO; diisopropylethylamine / CH₂Cl₂ / -78 - 20 °C

2.1: BuLi / tetrahydrofuran; hexane / -78 °C

2.2: 3.5 g / tetrahydrofuran; hexane

3.1: acetic acid; triflic acid / 0.5 h / ice bath

4.1: N,O-bis(trimethylsilyl)acetamide / acetonitrile / 0.75 h / Heating

4.2: TMSOTf / acetonitrile / 0 - 20 °C

With n-butyllithium; N,O-bis-(trimethylsilyl)-acetamide; oxalyl dichloride; trifluorormethanesulfonic acid; acetic acid; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; hexane; dichloromethane; acetonitrile; 1.1: Swern oxidation / 2.2: Wittig reaction / 4.2: Vorbrueggen reaction;
DOI:10.1021/ja071106y