Aminooxoessigsaeure-2-acetyl-2-methyl-1-phenylhydrazid

Base Information

• Chemical Name: Aminooxoessigsaeure-2-acetyl-2-methyl-1-phenylhydrazid
• CAS No.: 115177-49-6
• Molecular Formula: C₁₁H₁₃N₃O₃
• Molecular Weight: 235.243
• Mol file: 115177-49-6.mol

Synonyms:Aminooxoessigsaeure-2-acetyl-2-methyl-1-phenylhydrazid

Chemical Property of Aminooxoessigsaeure-2-acetyl-2-methyl-1-phenylhydrazid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Aminooxoessigsaeure-2-acetyl-2-methyl-1-phenylhydrazid

There total 2 articles about Aminooxoessigsaeure-2-acetyl-2-methyl-1-phenylhydrazid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

4-amino-2,3-dimethyl-1-phenylpyrazolin-5-one (83-07-8) → Aminooxoessigsaeure-2-acetyl-2-methyl-1-phenylhydrazid (115177-49-6)

Guidance literature:

With oxygen; methylene blue; at 20 ℃; for 2h; Irradiation;

DOI:10.1002/ardp.19883210109

Reference yield:

4-amino-2,3-dimethyl-1-phenylpyrazolin-5-one (83-07-8) → 1-acetyl-1-methyl-2-phenylhydrazine (38604-70-5) + Aminooxoessigsaeure-2-acetyl-2-methyl-1-phenylhydrazid (115177-49-6) + Oxalsaeure-mono(2-acetyl-2-methyl-1-phenyl)hydrazid (38988-02-2)

Guidance literature:

With sodium hydroxide; phosphate buffer; dihydrogen peroxide; In water; for 144h; Product distribution; Ambient temperature; var. of pH;

Reference yield:

Aminooxoessigsaeure-2-acetyl-2-methyl-1-phenylhydrazid (115177-49-6) → 1-acetyl-1-methyl-2-phenylhydrazine (38604-70-5)

Guidance literature:

With phosphate buffer; In water; at 37 ℃; for 72h; Product distribution; Rate constant; Kinetics; var. of pH;

upstream raw materials:

4-amino-2,3-dimethyl-1-phenylpyrazolin-5-one

Downstream raw materials:

1-acetyl-1-methyl-2-phenylhydrazine