1-[2-hydroxy-2-(4-methoxyphenyl)ethyl]-4-(4-naphthalen-1-yl-butyl)piperazine

Base Information

Chemical Name:1-[2-hydroxy-2-(4-methoxyphenyl)ethyl]-4-(4-naphthalen-1-yl-butyl)piperazine
CAS No.:385843-93-6
Molecular Formula:C₂₇H₃₄N₂O₂
Molecular Weight:418.579
Hs Code.:

Synonyms:1-[2-hydroxy-2-(4-methoxyphenyl)ethyl]-4-(4-naphthalen-1-yl-butyl)piperazine

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Chemical Property of 1-[2-hydroxy-2-(4-methoxyphenyl)ethyl]-4-(4-naphthalen-1-yl-butyl)piperazine

Chemical Property:

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Technology Process of 1-[2-hydroxy-2-(4-methoxyphenyl)ethyl]-4-(4-naphthalen-1-yl-butyl)piperazine

There total 3 articles about 1-[2-hydroxy-2-(4-methoxyphenyl)ethyl]-4-(4-naphthalen-1-yl-butyl)piperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 385843-92-5
1-[2-(4-methoxyphenyl)-2-oxoethyl]-4-(4-naphthalen-1-yl-butyl)piperazine

aqueous potassium hydroxide: aqueous potassium hydroxide

: 385843-93-6
1-[2-hydroxy-2-(4-methoxyphenyl)ethyl]-4-(4-naphthalen-1-yl-butyl)piperazine

Guidance literature:: With sodium borohydrid; In water;

Reference yield:

: 385843-92-5
1-[2-(4-methoxyphenyl)-2-oxoethyl]-4-(4-naphthalen-1-yl-butyl)piperazine

: 385843-93-6
1-[2-hydroxy-2-(4-methoxyphenyl)ethyl]-4-(4-naphthalen-1-yl-butyl)piperazine

Guidance literature:: With sodium hydroxide; sodium tetrahydroborate; In ethanol; water; at 50 ℃; for 1h;
DOI:10.1016/j.bmc.2006.12.039

Reference yield:

: 1-[4-(1-naphthyl)butyl]piperazine dihydrochloride

: 385843-93-6
1-[2-hydroxy-2-(4-methoxyphenyl)ethyl]-4-(4-naphthalen-1-yl-butyl)piperazine

Guidance literature:: Multi-step reaction with 2 steps

1: ethyldiisopropylamine / CHCl₃ / 3 h / Heating

2: NaBH₄; NaOH / ethanol; H₂O / 1 h / 50 °C

With sodium hydroxide; sodium tetrahydroborate; N-ethyl-N,N-diisopropylamine; In ethanol; chloroform; water;
DOI:10.1016/j.bmc.2006.12.039