1-Decanol, 10-chloro-

Base Information

• Chemical Name: 1-Decanol, 10-chloro-
• CAS No.: 51309-10-5
• Molecular Formula: C10H21ClO
• Molecular Weight: 192.729
• Hs Code.: 2905590090
• European Community (EC) Number: 257-129-2
• DSSTox Substance ID: DTXSID7068631
• Nikkaji Number: J261.687D
• Wikidata: Q72518180
• Mol file: 51309-10-5.mol

Synonyms:10-Chloro-1-decanol;10-Chlorodecan-1-ol;51309-10-5;1-Decanol, 10-chloro-;EINECS 257-129-2;C10H21ClO;10-chlorodecanol;10-chloro-decan-1-ol;10-Chlorodecan-1-ol #;SCHEMBL595431;10-Chloro-1-decanol, 90%;C10-H21-Cl-O;DTXSID7068631;BBL103510;MFCD00004748;STL557320;AKOS015913138;BS-16943;CS-0158370;FT-0721153

Chemical Property of 1-Decanol, 10-chloro-

Chemical Property:

• Vapor Pressure: 0.000476mmHg at 25°C
• Melting Point: 12-13 °C(lit.)
• Refractive Index: n20/D 1.46(lit.)
• Boiling Point: 279.7 °C at 760 mmHg
• PKA: 15.20±0.10(Predicted)
• Flash Point: 121.9 °C
• PSA: 20.23000
• Density: 0.951g/cm³
• LogP: 3.33830
• Storage Temp.: Sealed in dry,Room Temperature
• XLogP3: 3.8
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 9
• Exact Mass: 192.1280930
• Heavy Atom Count: 12
• Complexity: 76.2

Purity/Quality:

98%,99%, ^*data from raw suppliers

10-Chloro-1-decanol 90% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-37/39

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(CCCCCCl)CCCCO

Technology Process of 1-Decanol, 10-chloro-

There total 5 articles about 1-Decanol, 10-chloro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.8%

1-hydroxy-10-chloro-3-decyne → 10-chlorodecanol (51309-10-5)

Guidance literature:

With sodium tetrahydroborate; hydrogen; nickel diacetate; zinc(II) oxide; In ethanol; at 35 - 55 ℃; for 7h;

Reference yield: 72.0%

1,10-Decanediol (112-47-0) → 10-chlorodecanol (51309-10-5)

Guidance literature:

With hydrogenchloride; In octane; n-heptane; water; at 87 ℃; for 20h;

Reference yield:

diethyl sebacate (110-40-7) → 10-chlorodecanol (51309-10-5)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium; ethanol

2: HCl

With hydrogenchloride; ethanol; sodium;

upstream raw materials:

1,10-Decanediol

diethyl sebacate

Downstream raw materials:

10-fluoro-decan-1-ol

10-chlorodecanoic acid

dibutyl-(10-hydroxy-decyl)-amine

1-bromo-10-decanol

Refernces

• 1、 Iwasaki, Takanori,Terahigashi, Shohei,Wang, Yufei,Tanaka, Arisa,Zhao, Hanqing,Fujimoto, Yukari,Fukase, Koichi,Kambe, Nobuaki. "Synthesis of Cyclopropane Fatty Acids by C(sp3)?C(sp3) Cross-Coupling Reaction and Formal Synthesis of α-Mycolic Acid". . p. 3810 - 3817. Retrieved 2018/09/18.
• 2、 Karpinska,Lewandowska,Grodner. "Ethynylation of the ether derivatives of ω-haloalkanols with lithium acetylide-ethylenediamide complex". . p. 937 - 942. Retrieved 2007/10/03.