sodium tetrakis(3-chlorophenyl)borate

Base Information

• Chemical Name: sodium tetrakis(3-chlorophenyl)borate
• CAS No.: 54512-36-6
• Molecular Formula: C₂₄H₁₆BCl₄*Na
• Molecular Weight: 480.004

Synonyms:sodium tetrakis(3-chlorophenyl)borate

Chemical Property of sodium tetrakis(3-chlorophenyl)borate

Chemical Property:

Purity/Quality:

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Technology Process of sodium tetrakis(3-chlorophenyl)borate

There total 4 articles about sodium tetrakis(3-chlorophenyl)borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

sodium tetrafluoroborate (13755-29-8) + 1-bromo-3-chlorobenzene (108-37-2) → sodium tetrakis(3-chlorophenyl)borate (54512-36-6)

Guidance literature:

1-bromo-3-chlorobenzene; With iodine; magnesium; In diethyl ether; at 20 ℃; for 2.5h;

sodium tetrafluoroborate; In diethyl ether; at 20 ℃; for 42h;

In diethyl ether;

DOI:10.1021/ja905432x

Reference yield:

1-bromo-3-chlorobenzene (108-37-2) → sodium tetrakis(3-chlorophenyl)borate (54512-36-6)

Guidance literature:

With sodium tetrafluoroborate; iodine; magnesium; In tetrahydrofuran; at 20 ℃; Reflux;

DOI:10.1080/00397911003718086

Reference yield:

{(CH3)3NH}(1+)*{B(C6H4Cl)4}(1-)={(CH3)3NH}{B(C6H4Cl)4} (54512-38-8) + sodium methylate (124-41-4) → sodium tetrakis(3-chlorophenyl)borate (54512-36-6)

Guidance literature:

In methanol; pure product;

DOI:10.1016/S0003-2670(01)85480-5

upstream raw materials:

sodium tetrafluoroborate

1-bromo-3-chlorobenzene

magnesium

{(CH₃)3NH}⁽¹⁺⁾*{B(C₆H₄Cl)4}^(1-)={(CH₃)3NH}{B(C₆H₄Cl)4}

Downstream raw materials:

{(CH₃)3NH}⁽¹⁺⁾*{B(C₆H₄Cl)4}^(1-)={(CH₃)3NH}{B(C₆H₄Cl)4}

(R)-3-(3-chlorophenyl)-3-methylcyclohexanone

C₂₁H₁₉ClO

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