C₅₉H₁₀₇NO₁₃Si₂

Base Information

• Chemical Name: C₅₉H₁₀₇NO₁₃Si₂
• CAS No.: 134628-58-3
• Molecular Formula: C₅₉H₁₀₇NO₁₃Si₂
• Molecular Weight: 1094.67
• Mol file: 134628-58-3.mol

Synonyms:C₅₉H₁₀₇NO₁₃Si₂

Chemical Property of C₅₉H₁₀₇NO₁₃Si₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₉H₁₀₇NO₁₃Si₂

There total 11 articles about C₅₉H₁₀₇NO₁₃Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C36H65NO12 (37398-66-6) → C59H107NO13Si2 (134628-58-3)

Guidance literature:

Multi-step reaction with 10 steps

1: 95 percent / DMAP

2: NaBH₄ / methanol

3: H⁺

4: H₂ / 5percent Pd-C / ethanol

5: LiAlH₄

6: 1.) DMAP, 2.) NaH

7: DMAP

8: NaH, Bu₄NI

9: Et₃N

10: KH, 18-crown-6

With dmap; sodium tetrahydroborate; lithium aluminium tetrahydride; 18-crown-6 ether; hydrogen; hydrogen cation; tetra-(n-butyl)ammonium iodide; potassium hydride; sodium hydride; triethylamine; palladium on activated charcoal; In methanol; ethanol;

DOI:10.1021/ja00014a063

Reference yield:

erythromycin B (527-75-3,40627-91-6,57172-63-1,66101-02-8) → C59H107NO13Si2 (134628-58-3)

Guidance literature:

Multi-step reaction with 11 steps

1: 96 percent / I₂ / methanol / Irradiation

2: 95 percent / DMAP

3: NaBH₄ / methanol

4: H⁺

5: H₂ / 5percent Pd-C / ethanol

6: LiAlH₄

7: 1.) DMAP, 2.) NaH

8: DMAP

9: NaH, Bu₄NI

10: Et₃N

11: KH, 18-crown-6

With dmap; sodium tetrahydroborate; lithium aluminium tetrahydride; 18-crown-6 ether; hydrogen; iodine; hydrogen cation; tetra-(n-butyl)ammonium iodide; potassium hydride; sodium hydride; triethylamine; palladium on activated charcoal; In methanol; ethanol;

DOI:10.1021/ja00014a063

Reference yield:

C44H73NO14 → C59H107NO13Si2 (134628-58-3)

Guidance literature:

Multi-step reaction with 8 steps

1: H⁺

2: H₂ / 5percent Pd-C / ethanol

3: LiAlH₄

4: 1.) DMAP, 2.) NaH

5: DMAP

6: NaH, Bu₄NI

7: Et₃N

8: KH, 18-crown-6

With dmap; lithium aluminium tetrahydride; 18-crown-6 ether; hydrogen; hydrogen cation; tetra-(n-butyl)ammonium iodide; potassium hydride; sodium hydride; triethylamine; palladium on activated charcoal; In ethanol;

DOI:10.1021/ja00014a063

upstream raw materials:

methyl iodide

C₃₆H₆₅NO₁₂

erythromycin B

C₃₈H₆₉NO₁₂

Downstream raw materials:

C₄₇H₇₅NO₁₃

C₄₇H₇₇NO₁₄