1-methyl-3-buten-2-yl allyl ether

Base Information

• Chemical Name: 1-methyl-3-buten-2-yl allyl ether
• CAS No.: 63163-54-2
• Molecular Formula: C₈H₁₄O
• Molecular Weight: 126.199
• Mol file: 63163-54-2.mol

Synonyms:1-methyl-3-buten-2-yl allyl ether

Chemical Property of 1-methyl-3-buten-2-yl allyl ether

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 1-methyl-3-buten-2-yl allyl ether

There total 2 articles about 1-methyl-3-buten-2-yl allyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-chloro-3-methyl-1-butene (2190-48-9) + allyl alcohol (107-18-6) → 1-methyl-3-buten-2-yl allyl ether (63163-54-2) + isoprene (78-79-5,9003-31-0)

Guidance literature:

With 1,3,5-triphenylverdazyl; at 25 ℃; Kinetics;

DOI:10.1007/s11176-005-0441-5

Reference yield:

3-chloro-3-methyl-1-butene (2190-48-9) + 1,3,5-triphenylverdazyl (2154-65-6) + allyl alcohol (107-18-6) → 1-methyl-3-buten-2-yl allyl ether (63163-54-2) + 1,3,5-triphenylverdazylium chloride (72024-84-1) + 2,4,6-triphenylverdazyl (22459-57-0) + isoprene (78-79-5,9003-31-0)

Guidance literature:

at 22 ℃; Further Variations:; Temperatures; Kinetics;

DOI:10.1134/S1070363207070110

Reference yield: 84.0%

1-methyl-3-buten-2-yl allyl ether (63163-54-2) + p-methoxyphenylbutadiene (30448-78-3) → 1-((2Z)-5-{[(1,1-dimethylprop-2-en-1-yl)oxy]methyl}hexa-2,5-dien-1-yl)-4-methoxybenzene (1175163-89-9)

Guidance literature:

With cobalt(II) bromide-[1,2-bis(diphenylphosphino)ethane]; zinc(II) iodide; zinc; In dichloromethane; at 20 ℃; Inert atmosphere;

DOI:10.1021/ol901064p

upstream raw materials:

3-chloro-3-methyl-1-butene

allyl alcohol

1,3,5-triphenylverdazyl

Downstream raw materials:

6-methyl-hepta-1,5-dien-3-one

1-((2Z)-5-{[(1,1-dimethylprop-2-en-1-yl)oxy]methyl}hexa-2,5-dien-1-yl)-4-methoxybenzene