ADD 61060

Base Information

• Chemical Name: ADD 61060
• CAS No.: 97230-32-5
• Molecular Formula: C₁₃H₁₁FN₄
• Molecular Weight: 242.256

Synonyms:

Chemical Property of ADD 61060

Chemical Property:

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Technology Process of ADD 61060

There total 1 articles about ADD 61060 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

diazomethane (186581-53-3,908094-01-9,334-88-3) + 4-<(4-fluorophenyl)iminomethyl>pyridine (110684-46-3) → ADD 61060 (97230-32-5)

Guidance literature:

In 1,4-dioxane; water; Ambient temperature;

DOI:10.1021/jm00396a032

Reference yield: 77.8%

ADD 61060 (97230-32-5) → 4-[3-(4-Fluoro-phenyl)-3H-[1,2,3]triazol-4-yl]-pyridine (110684-22-5)

Guidance literature:

With nickel(IV) oxide; In benzene; for 3h; Heating;

DOI:10.1021/jo00310a022

Reference yield: 35.0%

ADD 61060 (97230-32-5) → (4-Fluoro-phenyl)-[1-pyridin-4-yl-eth-(Z)-ylidene]-amine

Guidance literature:

With potassium permanganate; tetrabutyl-ammonium chloride; In benzene; for 1h; Heating;

upstream raw materials:

diazomethane

4-<(4-fluorophenyl)iminomethyl>pyridine

Downstream raw materials:

4-[3-(4-Fluoro-phenyl)-3H-[1,2,3]triazol-4-yl]-pyridine

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