benzyl 4-(3-(3,4-bis(benzyloxy)phenyl)-N-(3-aminopropyl)propanamido)butyl(3-(3-(3,4-bis(benzyloxy)phenyl)propanamido)propyl)carbamate

Base Information

Chemical Name:benzyl 4-(3-(3,4-bis(benzyloxy)phenyl)-N-(3-aminopropyl)propanamido)butyl(3-(3-(3,4-bis(benzyloxy)phenyl)propanamido)propyl)carbamate
CAS No.:1375180-15-6
Molecular Formula:C₆₄H₇₂N₄O₈
Molecular Weight:1025.3
Hs Code.:

Synonyms:benzyl 4-(3-(3,4-bis(benzyloxy)phenyl)-N-(3-aminopropyl)propanamido)butyl(3-(3-(3,4-bis(benzyloxy)phenyl)propanamido)propyl)carbamate

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Chemical Property of benzyl 4-(3-(3,4-bis(benzyloxy)phenyl)-N-(3-aminopropyl)propanamido)butyl(3-(3-(3,4-bis(benzyloxy)phenyl)propanamido)propyl)carbamate

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Technology Process of benzyl 4-(3-(3,4-bis(benzyloxy)phenyl)-N-(3-aminopropyl)propanamido)butyl(3-(3-(3,4-bis(benzyloxy)phenyl)propanamido)propyl)carbamate

There total 12 articles about benzyl 4-(3-(3,4-bis(benzyloxy)phenyl)-N-(3-aminopropyl)propanamido)butyl(3-(3-(3,4-bis(benzyloxy)phenyl)propanamido)propyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1375180-12-3
C₆₄H₆₈N₄O₈

: 1375180-15-6
benzyl 4-(3-(3,4-bis(benzyloxy)phenyl)-N-(3-aminopropyl)propanamido)butyl(3-(3-(3,4-bis(benzyloxy)phenyl)propanamido)propyl)carbamate

Guidance literature:: With ammonia; hydrogen; In tetrahydrofuran; methanol; at 50 ℃; under 7500.75 - 15001.5 Torr; Autoclave;

Reference yield:

: 2107-70-2
3,4-methoxycinnamic acid

: 1375180-15-6
benzyl 4-(3-(3,4-bis(benzyloxy)phenyl)-N-(3-aminopropyl)propanamido)butyl(3-(3-(3,4-bis(benzyloxy)phenyl)propanamido)propyl)carbamate

Guidance literature:: Multi-step reaction with 6 steps

1: water; hydrogen bromide / 140 °C

2: potassium carbonate / N,N-dimethyl-formamide / 80 °C

3: sodium hydroxide; water / methanol / 90 °C / Reflux

4: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 5 h / 20 - 65 °C / Reflux

5: triethylamine / dichloromethane / 0 °C

6: ammonia; hydrogen / methanol; tetrahydrofuran / 50 °C / 7500.75 - 15001.5 Torr / Autoclave

With thionyl chloride; ammonia; water; hydrogen bromide; hydrogen; potassium carbonate; triethylamine; N,N-dimethyl-formamide; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1078-61-1
dihydrocaffeic acid

: 1375180-15-6
benzyl 4-(3-(3,4-bis(benzyloxy)phenyl)-N-(3-aminopropyl)propanamido)butyl(3-(3-(3,4-bis(benzyloxy)phenyl)propanamido)propyl)carbamate

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / N,N-dimethyl-formamide / 80 °C

2: sodium hydroxide; water / methanol / 90 °C / Reflux

3: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 5 h / 20 - 65 °C / Reflux

4: triethylamine / dichloromethane / 0 °C

5: ammonia; hydrogen / methanol; tetrahydrofuran / 50 °C / 7500.75 - 15001.5 Torr / Autoclave

With thionyl chloride; ammonia; water; hydrogen; potassium carbonate; triethylamine; N,N-dimethyl-formamide; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;