Technology Process of C44H36BF2N5S2
There total 6 articles about C44H36BF2N5S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
1,7-dithienyl-3,5-di(4-bromophenyl)borondifluoride-azadipyrromethene; 4-(dimethylamino)benzene-boronic acid;
With
sodium carbonate;
In
tetrahydrofuran; water; toluene;
for 0.0833333h;
Inert atmosphere;
With
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; water; toluene;
at 80 ℃;
DOI:10.1002/ejoc.201301300
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium hydroxide / ethanol / 20 °C
2.1: methanol / Reflux
3.1: ammonium acetate / butan-1-ol / 120 °C
4.1: N-ethyl-N,N-diisopropylamine / chloroform / 1 h
4.2: 20 °C
5.1: sodium carbonate / water; tetrahydrofuran; toluene / 0.08 h / Inert atmosphere
5.2: 80 °C
With
ammonium acetate; sodium carbonate; N-ethyl-N,N-diisopropylamine; potassium hydroxide;
In
tetrahydrofuran; methanol; ethanol; chloroform; water; toluene; butan-1-ol;
5.1: |Suzuki-Miyaura Coupling;
DOI:10.1002/ejoc.201301300
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: ammonium acetate / butan-1-ol / 120 °C
2.1: N-ethyl-N,N-diisopropylamine / chloroform / 1 h
2.2: 20 °C
3.1: sodium carbonate / water; tetrahydrofuran; toluene / 0.08 h / Inert atmosphere
3.2: 80 °C
With
ammonium acetate; sodium carbonate; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; chloroform; water; toluene; butan-1-ol;
3.1: |Suzuki-Miyaura Coupling;
DOI:10.1002/ejoc.201301300
