methyl 1-[(2S)-3-[(methylsulfonyl)oxy]-2-({[(phenylmethyl)oxy]carbonyl}amino)propyl]-L-prolinate

Base Information

Chemical Name:methyl 1-[(2S)-3-[(methylsulfonyl)oxy]-2-({[(phenylmethyl)oxy]carbonyl}amino)propyl]-L-prolinate
CAS No.:650578-05-5
Molecular Formula:C₁₈H₂₆N₂O₇S
Molecular Weight:414.48
Hs Code.:

Synonyms:methyl 1-[(2S)-3-[(methylsulfonyl)oxy]-2-({[(phenylmethyl)oxy]carbonyl}amino)propyl]-L-prolinate

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Chemical Property of methyl 1-[(2S)-3-[(methylsulfonyl)oxy]-2-({[(phenylmethyl)oxy]carbonyl}amino)propyl]-L-prolinate

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Technology Process of methyl 1-[(2S)-3-[(methylsulfonyl)oxy]-2-({[(phenylmethyl)oxy]carbonyl}amino)propyl]-L-prolinate

There total 4 articles about methyl 1-[(2S)-3-[(methylsulfonyl)oxy]-2-({[(phenylmethyl)oxy]carbonyl}amino)propyl]-L-prolinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 650577-98-3
methyl 1-[(2S)-3-hydroxy-2-({[(phenylmethyl)oxy]carbonyl}amino)propyl]-L-prolinate

: 124-63-0
methanesulfonyl chloride

: 650578-05-5
methyl 1-[(2S)-3-[(methylsulfonyl)oxy]-2-({[(phenylmethyl)oxy]carbonyl}amino)propyl]-L-prolinate

Guidance literature:: With dmap; triethylamine; at 0 ℃; for 1h;

Reference yield:

: 1,2-dideoxy-1-[(2S)-2-(methoxycarbonyl)-1-pyrrolidinyl]-2-[[(phenylmethoxy)carbonyl]amino]-D-glycero-hexitol

: 650578-05-5
methyl 1-[(2S)-3-[(methylsulfonyl)oxy]-2-({[(phenylmethyl)oxy]carbonyl}amino)propyl]-L-prolinate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium periodate / water / 20 h / 0 °C

1.2: 1 h / 0 °C

2.1: triethylamine; dmap / dichloromethane / 1 h / 0 °C

With dmap; sodium periodate; triethylamine; In dichloromethane; water;

Reference yield:

: 2133-40-6
L-proline methyl ester monohydrochloride

: 650578-05-5
methyl 1-[(2S)-3-[(methylsulfonyl)oxy]-2-({[(phenylmethyl)oxy]carbonyl}amino)propyl]-L-prolinate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium cyanoborohydride; methanol / 14 h / 64 °C

2.1: sodium periodate / water / 20 h / 0 °C

2.2: 1 h / 0 °C

3.1: triethylamine; dmap / dichloromethane / 1 h / 0 °C

With methanol; dmap; sodium periodate; sodium cyanoborohydride; triethylamine; In dichloromethane; water;