{4-[2-(S)-(4-ethylthiazol-2-yl)-2-(2-phenylacetylamido)ethyl]phenyl}sulfamic acid ammonium salt

Base Information

Chemical Name:{4-[2-(S)-(4-ethylthiazol-2-yl)-2-(2-phenylacetylamido)ethyl]phenyl}sulfamic acid ammonium salt
CAS No.:1235330-48-9
Molecular Formula:C₂₁H₂₃N₃O₄S₂*H₃N
Molecular Weight:462.594
Hs Code.:

Synonyms:{4-[2-(S)-(4-ethylthiazol-2-yl)-2-(2-phenylacetylamido)ethyl]phenyl}sulfamic acid ammonium salt

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Chemical Property of {4-[2-(S)-(4-ethylthiazol-2-yl)-2-(2-phenylacetylamido)ethyl]phenyl}sulfamic acid ammonium salt

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Technology Process of {4-[2-(S)-(4-ethylthiazol-2-yl)-2-(2-phenylacetylamido)ethyl]phenyl}sulfamic acid ammonium salt

There total 7 articles about {4-[2-(S)-(4-ethylthiazol-2-yl)-2-(2-phenylacetylamido)ethyl]phenyl}sulfamic acid ammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₁H₂₃N₃OS

: 1235330-48-9
{4-[2-(S)-(4-ethylthiazol-2-yl)-2-(2-phenylacetylamido)ethyl]phenyl}sulfamic acid ammonium salt

Guidance literature:: C₂₁H₂₃N₃OS; With pyridine-SO₃ complex; In pyridine; at 20 ℃; for 0.0833333h;

With ammonium hydroxide; In pyridine; water;

Reference yield:

: 1000394-26-2
N-[1-(4-ethylthiazol-2-yl)-2-(4-nitrophenyl)ethyl]-2-phenylacetamide

: 1235330-48-9
{4-[2-(S)-(4-ethylthiazol-2-yl)-2-(2-phenylacetylamido)ethyl]phenyl}sulfamic acid ammonium salt

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / methanol / 18 h

2: pyridine; sulfur trioxide pyridine complex / 0.08 h / 20 °C

With pyridine; hydrogen; sulfur trioxide pyridine complex; palladium 10% on activated carbon; In methanol;

Reference yield:

: 33305-77-0
Boc-Phe(p-NO₂)-OH

: 1235330-48-9
{4-[2-(S)-(4-ethylthiazol-2-yl)-2-(2-phenylacetylamido)ethyl]phenyl}sulfamic acid ammonium salt

Guidance literature:: Multi-step reaction with 6 steps

1.1: 4-methyl-morpholine; isobutyl chloroformate / N,N-dimethyl-formamide / 0.33 h / 0 °C

1.2: 0.5 h / 0 °C

2.1: Lawessons reagent / tetrahydrofuran / 3 h / 20 °C

3.1: acetonitrile / 3 h / Reflux

4.1: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 0 - 20 °C

5.1: hydrogen / palladium 10% on activated carbon / methanol / 18 h

6.1: pyridine; sulfur trioxide pyridine complex / 0.08 h / 20 °C

With Lawessons reagent; 4-methyl-morpholine; pyridine; hydrogen; sulfur trioxide pyridine complex; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; isobutyl chloroformate; palladium 10% on activated carbon; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetonitrile;