β-(4-Hydroxy)phenylethyl nonanoate

Base Information

• Chemical Name: β-(4-Hydroxy)phenylethyl nonanoate
• CAS No.: 137422-38-9
• Molecular Formula: C₁₇H₂₆O₃
• Molecular Weight: 278.392
• Mol file: 137422-38-9.mol

Synonyms:β-(4-Hydroxy)phenylethyl nonanoate

Chemical Property of β-(4-Hydroxy)phenylethyl nonanoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of β-(4-Hydroxy)phenylethyl nonanoate

There total 5 articles about β-(4-Hydroxy)phenylethyl nonanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.5%

β-(4-Benzyloxy)phenylethyl nonanoate (137422-37-8) → β-(4-Hydroxy)phenylethyl nonanoate (137422-38-9)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; at 30 ℃; for 1h; under 2792.6 Torr;

Reference yield:

2-[4-(benzyloxy)benzyl]acetic acid (6547-53-1) → β-(4-Hydroxy)phenylethyl nonanoate (137422-38-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 92.7 percent / BH₃ / tetrahydrofuran

2: Et₃N

3: 96.5 percent / H₂ / 5percent Pd/C / ethanol / 1 h / 30 °C / 2792.6 Torr

With borane; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol;

Reference yield:

2-(4-(benzyloxy)phenyl)acetyl chloride (39188-62-0) → β-(4-Hydroxy)phenylethyl nonanoate (137422-38-9)

Guidance literature:

Multi-step reaction with 4 steps

1: Et₃N / CH₂Cl₂ / 1) room temp., 17 h, 2) reflux, 1 h

2: 90.3 percent / LAH / diethyl ether / 21 h / Heating

3: Et₃N

4: 96.5 percent / H₂ / 5percent Pd/C / ethanol / 1 h / 30 °C / 2792.6 Torr

With lithium aluminium tetrahydride; hydrogen; triethylamine; palladium on activated charcoal; In diethyl ether; ethanol; dichloromethane;

upstream raw materials:

β-(4-Benzyloxy)phenylethyl nonanoate

2-(4-benzyloxyphenyl)ethanol

2-(4-(benzyloxy)phenyl)acetyl chloride

2-[4-(benzyloxy)benzyl]acetic acid

Downstream raw materials:

4-Hexyloxy-benzoic acid 4-(2-nonanoyloxy-ethyl)-phenyl ester

4-Dodecyloxy-benzoic acid 4-(2-nonanoyloxy-ethyl)-phenyl ester

4-Decyloxy-benzoic acid 4-(2-nonanoyloxy-ethyl)-phenyl ester

4-Octyloxy-benzoic acid 4-(2-nonanoyloxy-ethyl)-phenyl ester

Refernces