NiCO(1,10-diphospha⁽²⁾-2,6-pyridino⁽²⁾-1,1'-ferrocenophane

Base Information

Chemical Name:NiCO(1,10-diphospha⁽²⁾-2,6-pyridino⁽²⁾-1,1'-ferrocenophane
CAS No.:540743-27-9
Molecular Formula:C₃₈H₆₉FeNNiOP₂Si₆
Molecular Weight:900.969
Hs Code.:

NiCO(1,10-diphospha<sup>(2)</sup>-2,6-pyridino<sup>(2)</sup>-1,1'-ferrocenophane

Synonyms:NiCO(1,10-diphospha⁽²⁾-2,6-pyridino⁽²⁾-1,1'-ferrocenophane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of NiCO(1,10-diphospha⁽²⁾-2,6-pyridino⁽²⁾-1,1'-ferrocenophane

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Technology Process of NiCO(1,10-diphospha⁽²⁾-2,6-pyridino⁽²⁾-1,1'-ferrocenophane

There total 1 articles about NiCO(1,10-diphospha⁽²⁾-2,6-pyridino⁽²⁾-1,1'-ferrocenophane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 540743-24-6
1,10-diphospha⁽²⁾-2,6-pyridino⁽²⁾-1,1'-ferrocenophane

: 13463-39-3,71564-36-8
tetracarbonyl nickel

: 540743-27-9
NiCO(1,10-diphospha⁽²⁾-2,6-pyridino⁽²⁾-1,1'-ferrocenophane

Guidance literature:: In diethyl ether; at -30 °C Ni(CO)4 added dropwise to soln. of Fe(C5H4)2C5H3N(CHSi(CH3)3PCH(Si(CH3)3)2)2 in diethyl ether, soln. stirred for 12 h at room temp.; excess of Ni(CO)4 and solvent removed under reduced pressure, residue dissolved in small amount of diethyl ether, at 0 °C crystd. within two days;
DOI:10.1002/anie.200390132