C₁₁H₁₂O

Base Information

• Chemical Name: C₁₁H₁₂O
• CAS No.: 1379615-13-0
• Molecular Formula: C₁₁H₁₂O
• Molecular Weight: 160.216
• Mol file: 1379615-13-0.mol

Synonyms:C₁₁H₁₂O

Chemical Property of C₁₁H₁₂O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₁₁H₁₂O

There total 1 articles about C₁₁H₁₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

acrylaldehyde diethyl acetal (3054-95-3) → C11H12O (1379615-13-0)

Guidance literature:

With potassium chloride; tetrabutylammonium acetate; palladium diacetate; potassium carbonate; In N,N-dimethyl-formamide; at 90 ℃; for 3h;

DOI:10.1002/cjoc.201800205

Reference yield: 94.0%

C11H12O (1379615-13-0) + Methyltriphenylphosphonium bromide (1779-49-3) → (E)-1-(buta-1,3-dien-1-yl)-3,5-dimethylbenzene

Guidance literature:

Methyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 0.5h; Inert atmosphere;

C₁₁H₁₂O; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 3h; Inert atmosphere;

DOI:10.1002/cjoc.201800205

Reference yield: 84.0%

C11H12O (1379615-13-0) + C16H10FIOS → (aR)-3-(3,5-dimethylphenyl)-4-(2-fluoro-6-iodophenyl)dibenzo[b,d]thiophene

Guidance literature:

C₁₁H₁₂O; C₁₆H₁₀FIOS; With (5aR,10bS)-2-mesityl-5a,10b-dihydro-4H,6H-indeno[2,1-b][1,2,4]triazolo[4,3-d][1,4]oxazin-2-ium tetrafluoroborate; 3,5,3',5'-tetra-tert-butyl-4,4'-diphenoquinone; 1,8-diazabicyclo[5.4.0]undec-7-ene; In 1,2-dichloro-ethane; at -10 ℃; Schlenk technique; Inert atmosphere; Sealed tube;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 1,2-dichloro-ethane; at -10 ℃; for 0.666667h; enantioselective reaction; Schlenk technique; Inert atmosphere; Sealed tube;

DOI:10.1002/anie.202103415

upstream raw materials:

acrylaldehyde diethyl acetal

Downstream raw materials:

methyl (1R,2S,3R,10bR)-2-(3,5-dimethylphenyl)-1-[(1E)-3-ethoxy-3-oxoprop-1-en-1-yl]-8,9-dimethoxy-3-methyl-1,2,3,5,6,10b-hexahydropyrrolo[2,1-a]isoquinoline-3-carboxylate

dimethyl (2S,3S,12bR)-[2-(3,5-dimethylphenyl)-4-oxo-1,2,3,4,6,7,12,12b-octahydroindolo[2,3-a]quinolizin-3-yl]phosphonate

(S)-4-(3,5-dimethylphenyl)-1-methyl-3-methylenepiperidin-2-one