methyl DL-2,3-bis[((triphenylmethyl)thio)-acetamido]propionate

Base Information

Chemical Name:methyl DL-2,3-bis[((triphenylmethyl)thio)-acetamido]propionate
CAS No.:224184-31-0
Molecular Formula:C₄₆H₄₂N₂O₄S₂
Molecular Weight:750.982
Hs Code.:

Synonyms:methyl DL-2,3-bis[((triphenylmethyl)thio)-acetamido]propionate

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Chemical Property of methyl DL-2,3-bis[((triphenylmethyl)thio)-acetamido]propionate

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Technology Process of methyl DL-2,3-bis[((triphenylmethyl)thio)-acetamido]propionate

There total 4 articles about methyl DL-2,3-bis[((triphenylmethyl)thio)-acetamido]propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 91425-31-9
2-(triphenylmethylthio)ethanoic acid-N-hydroxysuccinimido ester

: methyl 2,3-diaminopropanoate p-toluenesulfonate

: 224184-31-0
methyl DL-2,3-bis[((triphenylmethyl)thio)-acetamido]propionate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 8h; Heating;
DOI:10.1139/v98-220

Reference yield: 57.0%

: 34914-36-8
2-(triphenylmethylthio)ethanoic acid

: 6059-44-5,106973-48-2,147857-43-0
methyl 2,3-diaminopropanoate dihydrochloride

: 224184-31-0
methyl DL-2,3-bis[((triphenylmethyl)thio)-acetamido]propionate

Guidance literature:: methyl 2,3-diaminopropanoate dihydrochloride; With potassium hydroxide; In methanol; for 0.0833333h;

2-(triphenylmethylthio)ethanoic acid; With 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; for 1h;

Reference yield:

: 76-84-6
triphenylmethyl alcohol

: 224184-31-0
methyl DL-2,3-bis[((triphenylmethyl)thio)-acetamido]propionate

Guidance literature:: Multi-step reaction with 3 steps

1.1: boron trifluoride diethyl etherate / chloroform / 20 °C

2.1: potassium hydroxide; water / methanol

2.2: pH 6

3.1: potassium hydroxide / methanol / 0.08 h

3.2: 1 h

With boron trifluoride diethyl etherate; water; potassium hydroxide; In methanol; chloroform;