[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl] 2-oxocycloheptanecarboxylate

Base Information

Chemical Name:[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl] 2-oxocycloheptanecarboxylate
CAS No.:1146352-83-1
Molecular Formula:C₂₄H₃₄O₃
Molecular Weight:370.532
Hs Code.:

Synonyms:[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl] 2-oxocycloheptanecarboxylate

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Chemical Property of [(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl] 2-oxocycloheptanecarboxylate

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Technology Process of [(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl] 2-oxocycloheptanecarboxylate

There total 2 articles about [(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl] 2-oxocycloheptanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 52784-32-4
2-(methoxycarbonyl)cycloheptanone

: 65253-04-5
(-)-8-phenylmenthol

: 1146352-83-1
[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl] 2-oxocycloheptanecarboxylate

Guidance literature:: With dmap; In toluene; for 48h; Inert atmosphere; Reflux;
DOI:10.1021/ol9003405

Reference yield:

: 65253-04-5
(-)-8-phenylmenthol

: 108-24-7
acetic anhydride

: 502-42-1
cycloheptanone

: 1146352-83-1
[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl] 2-oxocycloheptanecarboxylate

Guidance literature:: acetic anhydride; cycloheptanone; With sodium hydride; In mineral oil; benzene; for 7h; Inert atmosphere; Reflux;

(-)-8-phenylmenthol; With dmap; In toluene; for 96h; Inert atmosphere; Reflux;
DOI:10.1021/acs.orglett.8b01087

Reference yield: 62.0%

: 1146352-83-1
[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl] 2-oxocycloheptanecarboxylate

: 1146352-87-5
[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl] 7-oxocyclohept-1-enecarboxylate

Guidance literature:: [(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl] 2-oxocycloheptanecarboxylate; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.166667h; Inert atmosphere;

With N-(tert-butyl)benzenesulfinimidoyl chloride; In tetrahydrofuran; for 0.666667h; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol9003405