tert-Butyl{3-[4-(3,4-dichlorobenzyloxy)phenyl]-3-vinyloxypropoxy}dimethylsilane

Base Information

Chemical Name:tert-Butyl{3-[4-(3,4-dichlorobenzyloxy)phenyl]-3-vinyloxypropoxy}dimethylsilane
CAS No.:1202577-17-0
Molecular Formula:C₂₄H₃₂Cl₂O₃Si
Molecular Weight:467.508
Hs Code.:

Synonyms:tert-Butyl{3-[4-(3,4-dichlorobenzyloxy)phenyl]-3-vinyloxypropoxy}dimethylsilane

Suppliers and Price of tert-Butyl{3-[4-(3,4-dichlorobenzyloxy)phenyl]-3-vinyloxypropoxy}dimethylsilane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tert-Butyl{3-[4-(3,4-dichlorobenzyloxy)phenyl]-3-vinyloxypropoxy}dimethylsilane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tert-Butyl{3-[4-(3,4-dichlorobenzyloxy)phenyl]-3-vinyloxypropoxy}dimethylsilane

There total 4 articles about tert-Butyl{3-[4-(3,4-dichlorobenzyloxy)phenyl]-3-vinyloxypropoxy}dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1202577-14-7
3-(tert-butyldimethylsilyloxy)-1-[4-(3,4-dichloro benzyloxy)phenyl]propan-1-ol

: 1662-01-7
bathophenanthroline

: 1202577-17-0
tert-Butyl{3-[4-(3,4-dichlorobenzyloxy)phenyl]-3-vinyloxypropoxy}dimethylsilane

Guidance literature:: With triethylamine; palladium(II) trifluoroacetate; In -butyl vinyl ether; at 80 ℃; for 4h; Inert atmosphere;

Reference yield:

: 106-41-2
4-bromo-phenol

: 1202577-17-0
tert-Butyl{3-[4-(3,4-dichlorobenzyloxy)phenyl]-3-vinyloxypropoxy}dimethylsilane

Guidance literature:: Multi-step reaction with 3 steps

1.1: triphenylphosphine; diethylazodicarboxylate / toluene; tetrahydrofuran / 20 °C

2.1: n-butyllithium / hexane; tetrahydrofuran / -78 °C / Inert atmosphere

2.2: 0.08 h / -78 °C

3.1: triethylamine / palladium(II) trifluoroacetate / -butyl vinyl ether / 4 h / 80 °C / Inert atmosphere

With n-butyllithium; triethylamine; triphenylphosphine; diethylazodicarboxylate; palladium(II) trifluoroacetate; In tetrahydrofuran; -butyl vinyl ether; hexane; toluene;

Reference yield:

: 1805-32-9
3,4-dichlorobenzyl alcohol

: 1202577-17-0
tert-Butyl{3-[4-(3,4-dichlorobenzyloxy)phenyl]-3-vinyloxypropoxy}dimethylsilane

Guidance literature:: Multi-step reaction with 3 steps

1.1: triphenylphosphine; diethylazodicarboxylate / toluene; tetrahydrofuran / 20 °C

2.1: n-butyllithium / hexane; tetrahydrofuran / -78 °C / Inert atmosphere

2.2: 0.08 h / -78 °C

3.1: triethylamine / palladium(II) trifluoroacetate / -butyl vinyl ether / 4 h / 80 °C / Inert atmosphere

With n-butyllithium; triethylamine; triphenylphosphine; diethylazodicarboxylate; palladium(II) trifluoroacetate; In tetrahydrofuran; -butyl vinyl ether; hexane; toluene;