2-[2-(2-azidoethoxy)ethoxy]ethyl (2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside

Base Information

Chemical Name:2-[2-(2-azidoethoxy)ethoxy]ethyl (2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside
CAS No.:153253-42-0
Molecular Formula:C₃₂H₄₇N₃O₂₀
Molecular Weight:793.733
Hs Code.:

Synonyms:2-[2-(2-azidoethoxy)ethoxy]ethyl (2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside

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Chemical Property of 2-[2-(2-azidoethoxy)ethoxy]ethyl (2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside

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Technology Process of 2-[2-(2-azidoethoxy)ethoxy]ethyl (2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside

There total 2 articles about 2-[2-(2-azidoethoxy)ethoxy]ethyl (2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 86520-52-7
2-[2-(2-azidoethoxy)ethoxy]ethanol

: 4753-07-5
2,3,6,2',3',4',6'-hepta-O-acetyl-lactosyl bromide

: 153253-42-0
2-[2-(2-azidoethoxy)ethoxy]ethyl (2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside

Guidance literature:: With mercury dibromide; mercury(II) oxide; In chloroform; at 20 ℃; for 48h;
DOI:10.1016/S0968-0896(99)00099-1

Reference yield: 65.0%

: 86520-52-7
2-[2-(2-azidoethoxy)ethoxy]ethanol

: 92052-38-5,106256-81-9,106256-89-7,126736-02-5,130703-21-8,132287-70-8,132287-71-9,139403-73-9
O-<2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-α,β-D-glucopyranosyl>trichloroacetimidate

: 153253-42-0
2-[2-(2-azidoethoxy)ethoxy]ethyl (2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; Molecular sieve;
DOI:10.1039/c3cc45147j

Reference yield: 92.0%

: 85-44-9
phthalic anhydride

: 153253-42-0
2-[2-(2-azidoethoxy)ethoxy]ethyl (2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside

: 733051-82-6
8-phthalimido-3,6-dioxaoctyl 4-O-(β-D-galactooyranosyl)-β-D-glucopyranoside

Guidance literature:: With chloro-trimethyl-silane; tetra-(n-butyl)ammonium iodide; sodium iodide; In acetonitrile; at 20 ℃; for 1h;
DOI:10.1016/j.carres.2004.03.032