dimethyl (Z)-2-[1-(tert-butylamino)-3-oxo-3-phenylprop-1-en-2-yl]but-2-enedioate

Base Information

Chemical Name:dimethyl (Z)-2-[1-(tert-butylamino)-3-oxo-3-phenylprop-1-en-2-yl]but-2-enedioate
CAS No.:1418127-00-0
Molecular Formula:C₁₉H₂₃NO₅
Molecular Weight:345.395
Hs Code.:

Synonyms:dimethyl (Z)-2-[1-(tert-butylamino)-3-oxo-3-phenylprop-1-en-2-yl]but-2-enedioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimethyl (Z)-2-[1-(tert-butylamino)-3-oxo-3-phenylprop-1-en-2-yl]but-2-enedioate

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Technology Process of dimethyl (Z)-2-[1-(tert-butylamino)-3-oxo-3-phenylprop-1-en-2-yl]but-2-enedioate

There total 1 articles about dimethyl (Z)-2-[1-(tert-butylamino)-3-oxo-3-phenylprop-1-en-2-yl]but-2-enedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14376-91-1
C₁₃H₁₇NO

: 762-42-5
dimethyl acetylenedicarboxylate

: 1418127-00-0
dimethyl (Z)-2-[1-(tert-butylamino)-3-oxo-3-phenylprop-1-en-2-yl]but-2-enedioate

: 1418126-99-4
dimethyl (E)-2-[1-(tert-butylamino)-3-oxo-3-phenylprop-1-en-2-yl]but-2-enedioate

Guidance literature:: With copper(l) iodide; In acetonitrile; at 20 ℃; for 20h; Overall yield = 60 %; Overall yield = 0.104 g; regioselective reaction; Inert atmosphere;
DOI:10.1055/s-0032-1317178

Reference yield: 33.0%

: 1418127-00-0
dimethyl (Z)-2-[1-(tert-butylamino)-3-oxo-3-phenylprop-1-en-2-yl]but-2-enedioate

: 762-42-5
dimethyl acetylenedicarboxylate

: 1418126-85-8
methyl 5-benzoyl-1-tert-butyl-2-oxo-1,2-dihydropyridine-4-carboxylate

Guidance literature:: With copper(l) iodide; In acetonitrile; at 120 ℃; for 3h; regioselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1055/s-0032-1317178