C₉H₉BrN₂

Base Information

Chemical Name:C₉H₉BrN₂
CAS No.:1398718-23-4
Molecular Formula:C₉H₉BrN₂
Molecular Weight:225.088
Hs Code.:

C<sub>9</sub>H<sub>9</sub>BrN<sub>2</sub>

Synonyms:C₉H₉BrN₂

Suppliers and Price of C₉H₉BrN₂

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Chemical Property of C₉H₉BrN₂

Chemical Property:

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Technology Process of C₉H₉BrN₂

There total 5 articles about C₉H₉BrN₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24250-84-8
H-p-BrPhe-OH

: 1398718-23-4
C₉H₉BrN₂

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride / Reflux

2: sodium hydrogencarbonate / acetone / 20 °C

3: ammonia; methanol / 0.25 h / -50 - 20 °C

4: triethylamine; trifluoroacetic anhydride / dichloromethane / 3.5 h / 0 - 20 °C / Inert atmosphere

5: formic acid / 4 h / 40 °C

With methanol; formic acid; thionyl chloride; ammonia; sodium hydrogencarbonate; triethylamine; trifluoroacetic anhydride; In dichloromethane; acetone;

Reference yield:

: 62129-39-9,79561-82-3
4-bromo-N-{[(1,1-dimethylethyl)oxy]carbonyl}-L-phenylalanine

: 1398718-23-4
C₉H₉BrN₂

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 20 °C

2: ammonia; methanol / 0.25 h / -50 - 20 °C

3: triethylamine; trifluoroacetic anhydride / dichloromethane / 3.5 h / 0 - 20 °C / Inert atmosphere

4: formic acid / 4 h / 40 °C

With methanol; formic acid; ammonia; potassium carbonate; triethylamine; trifluoroacetic anhydride; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 266306-18-7
(S)-3-(4-Bromo-phenyl)-2-tert-butoxycarbonylamino-propionic acid methyl ester

: 1398718-23-4
C₉H₉BrN₂

Guidance literature:: Multi-step reaction with 3 steps

1: ammonia; methanol / 0.25 h / -50 - 20 °C

2: triethylamine; trifluoroacetic anhydride / dichloromethane / 3.5 h / 0 - 20 °C / Inert atmosphere

3: formic acid / 4 h / 40 °C

With methanol; formic acid; ammonia; triethylamine; trifluoroacetic anhydride; In dichloromethane;