9-[8',8'-difluoro-8'-(diethylphosphono)oct-1'-ynyl]-2-N-(N,N-dimethylaminomethylidene)-7-N-(2-nitrophenyl)sulfonyl-1N-(pivaloyloxy)methyl-9-deazaguanine

Base Information

Chemical Name:9-[8',8'-difluoro-8'-(diethylphosphono)oct-1'-ynyl]-2-N-(N,N-dimethylaminomethylidene)-7-N-(2-nitrophenyl)sulfonyl-1N-(pivaloyloxy)methyl-9-deazaguanine
CAS No.:1225194-28-4
Molecular Formula:C₃₃H₄₃F₂N₆O₁₀PS
Molecular Weight:784.775
Hs Code.:

9-[8',8'-difluoro-8'-(diethylphosphono)oct-1'-ynyl]-2-N-(N,N-dimethylaminomethylidene)-7-N-(2-nitrophenyl)sulfonyl-1N-(pivaloyloxy)methyl-9-deazaguanine

Synonyms:9-[8',8'-difluoro-8'-(diethylphosphono)oct-1'-ynyl]-2-N-(N,N-dimethylaminomethylidene)-7-N-(2-nitrophenyl)sulfonyl-1N-(pivaloyloxy)methyl-9-deazaguanine

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Chemical Property of 9-[8',8'-difluoro-8'-(diethylphosphono)oct-1'-ynyl]-2-N-(N,N-dimethylaminomethylidene)-7-N-(2-nitrophenyl)sulfonyl-1N-(pivaloyloxy)methyl-9-deazaguanine

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Technology Process of 9-[8',8'-difluoro-8'-(diethylphosphono)oct-1'-ynyl]-2-N-(N,N-dimethylaminomethylidene)-7-N-(2-nitrophenyl)sulfonyl-1N-(pivaloyloxy)methyl-9-deazaguanine

There total 1 articles about 9-[8',8'-difluoro-8'-(diethylphosphono)oct-1'-ynyl]-2-N-(N,N-dimethylaminomethylidene)-7-N-(2-nitrophenyl)sulfonyl-1N-(pivaloyloxy)methyl-9-deazaguanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1225194-25-1
diethyl 1,1-difluorooct-7-ynylphosphonate

: 1225194-14-8
2N-((N,N-dimethylamino)methylidene)-9-iodo-7N-(2-nitrophenylsulfonyl)-1N-(pivaloyloxy)methyl-9-deazaguanine

: 1225194-28-4
9-[8',8'-difluoro-8'-(diethylphosphono)oct-1'-ynyl]-2-N-(N,N-dimethylaminomethylidene)-7-N-(2-nitrophenyl)sulfonyl-1N-(pivaloyloxy)methyl-9-deazaguanine

Guidance literature:: diethyl 1,1-difluorooct-7-ynylphosphonate; With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In acetonitrile; at 20 ℃; for 1h; Inert atmosphere;

2N-((N,N-dimethylamino)methylidene)-9-iodo-7N-(2-nitrophenylsulfonyl)-1N-(pivaloyloxy)methyl-9-deazaguanine; In acetonitrile; at 60 ℃; for 15h; Inert atmosphere;
DOI:10.1016/j.bmc.2010.01.062