4-Phenyl-2,6,7-trioxa-1-phosphabicyclo[2.2.2]octane1-oxide

Base Information

Chemical Name:4-Phenyl-2,6,7-trioxa-1-phosphabicyclo[2.2.2]octane1-oxide
CAS No.:2200-87-5
Molecular Formula:C10H11 O4 P
Molecular Weight:226.1657
Hs Code.:2902909090
Mol file:2200-87-5.mol

Synonyms:1,3-Propanediol,2-(hydroxymethyl)-2-phenyl-, cyclic phosphate (7CI,8CI)

Suppliers and Price of 4-Phenyl-2,6,7-trioxa-1-phosphabicyclo[2.2.2]octane1-oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 4-Phenyl-2,6,7-trioxa-1-phosphabicyclo[2.2.2]octane1-oxide

Chemical Property:

Vapor Pressure:0.000639mmHg at 25°C
Boiling Point:319.3°Cat760mmHg
Flash Point:160.7°C
PSA：54.57000
Density:1.38g/cm³
LogP:2.10950

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-Phenyl-2,6,7-trioxa-1-phosphabicyclo[2.2.2]octane1-oxide

There total 5 articles about 4-Phenyl-2,6,7-trioxa-1-phosphabicyclo[2.2.2]octane1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53845-36-6
4-phenyl-2,6,7-trioxa-1-phosphabicyclo[2.2.2]octane

: 2200-87-5
4-Phenyl-2,6,7-trioxa-1-phosphabicyclo<2.2.2>octane 1-oxide

Guidance literature:: With dinitrogen tetraoxide; In chloroform; at 0 ℃;

Reference yield:

: 160820-67-7
2-Benzyloxymethyl-2-phenyl-propane-1,3-diol

: 2200-87-5
4-Phenyl-2,6,7-trioxa-1-phosphabicyclo<2.2.2>octane 1-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / Pd-C / ethanol / 760 Torr / Ambient temperature

2: P(OEt)3

3: N₂O₄ / CHCl₃ / 0 °C

With hydrogen; dinitrogen tetraoxide; triethyl phosphite; palladium on activated charcoal; In ethanol; chloroform;

Reference yield:

: 67590-44-7
2-Benzyloxymethyl-2-phenyl-malonic acid diethyl ester

: 2200-87-5
4-Phenyl-2,6,7-trioxa-1-phosphabicyclo<2.2.2>octane 1-oxide

Guidance literature:: Multi-step reaction with 4 steps

1: LiAlH₄ / diethyl ether / 2 h / Heating

2: H₂ / Pd-C / ethanol / 760 Torr / Ambient temperature

3: P(OEt)3

4: N₂O₄ / CHCl₃ / 0 °C

With lithium aluminium tetrahydride; hydrogen; dinitrogen tetraoxide; triethyl phosphite; palladium on activated charcoal; In diethyl ether; ethanol; chloroform;