1-Tosyldiazoethan

Base Information

Chemical Name:1-Tosyldiazoethan
CAS No.:42251-17-2
Molecular Formula:C₉H₁₀N₂O₂S
Molecular Weight:210.257
Hs Code.:

Synonyms:1-Tosyldiazoethan

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Chemical Property of 1-Tosyldiazoethan

Chemical Property:

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Technology Process of 1-Tosyldiazoethan

There total 4 articles about 1-Tosyldiazoethan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.6%

: 42251-16-1
C₁₂H₁₆N₂O₅S

: 42251-17-2
1-Tosyldiazoethan

Guidance literature:: With aluminum oxide; at 300 ℃;
DOI:10.1016/S0040-4039(00)00763-2

Reference yield:

: 3696-58-0
α-Methyl-N--urethan

: 42251-17-2
1-Tosyldiazoethan

Guidance literature:: Multi-step reaction with 2 steps

1: 61.2 percent / i-amyl nitrite; pyridine; TMSCl / CH₂Cl₂ / 20 °C

2: 72.6 percent / basic alumina / 300 °C

With pyridine; aluminum oxide; chloro-trimethyl-silane; isopentyl nitrite; In dichloromethane; 1: nitrosylation / 2: Diazotization;
DOI:10.1016/S0040-4039(00)00763-2

Reference yield:

: 824-79-3
sodium 4-methylbenzenesulfinate

: 42251-17-2
1-Tosyldiazoethan

Guidance literature:: Multi-step reaction with 3 steps

2: 61.2 percent / i-amyl nitrite; pyridine; TMSCl / CH₂Cl₂ / 20 °C

3: 72.6 percent / basic alumina / 300 °C

With pyridine; aluminum oxide; chloro-trimethyl-silane; isopentyl nitrite; In dichloromethane; 1: Condensation / 2: nitrosylation / 3: Diazotization;
DOI:10.1016/S0040-4039(00)00763-2