[4,4,4,5,5,5-hexacarbonyl-2,3,6-triphenyl-2,3,6-triphospha-4,5-diferratetracyclo[5.4.0.0(3,5).0(4,6).]undeca7⁽¹⁾,8,10-triene]tetracarbonyliron

Base Information

• Chemical Name: [4,4,4,5,5,5-hexacarbonyl-2,3,6-triphenyl-2,3,6-triphospha-4,5-diferratetracyclo[5.4.0.0(3,5).0(4,6).]undeca7⁽¹⁾,8,10-triene]tetracarbonyliron
• CAS No.: 89210-02-6
• Molecular Formula: C₃₄H₁₉Fe₃O₁₀P₃
• Molecular Weight: 847.981

Synonyms:[4,4,4,5,5,5-hexacarbonyl-2,3,6-triphenyl-2,3,6-triphospha-4,5-diferratetracyclo[5.4.0.0(3,5).0(4,6).]undeca7⁽¹⁾,8,10-triene]tetracarbonyliron

Chemical Property of [4,4,4,5,5,5-hexacarbonyl-2,3,6-triphenyl-2,3,6-triphospha-4,5-diferratetracyclo[5.4.0.0(3,5).0(4,6).]undeca7⁽¹⁾,8,10-triene]tetracarbonyliron

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Technology Process of [4,4,4,5,5,5-hexacarbonyl-2,3,6-triphenyl-2,3,6-triphospha-4,5-diferratetracyclo[5.4.0.0(3,5).0(4,6).]undeca7⁽¹⁾,8,10-triene]tetracarbonyliron

There total 2 articles about [4,4,4,5,5,5-hexacarbonyl-2,3,6-triphenyl-2,3,6-triphospha-4,5-diferratetracyclo[5.4.0.0(3,5).0(4,6).]undeca7⁽¹⁾,8,10-triene]tetracarbonyliron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

diiron nonacarbonyl (15321-51-4) + 1,2,3-triphenyl-1,2,3-triphosphaindane (89104-79-0,57194-41-9,5994-68-3) → [4,4,4,5,5,5-hexacarbonyl-2,3,6-triphenyl-2,3,6-triphospha-4,5-diferratetracyclo[5.4.0.0(3,5).0(4,6).]undeca7(1),8,10-triene]tetracarbonyliron (89210-02-6) + 3,3,3,4,4,4,6,6,6-nonacarbonyl-2,5,7-triphenyl-2,5,7-triphospha-3,4,6-triferrapentacyclo[6.4.0.0(2,6).0(3,5).0(4,7).]dodeca-8(1),9,11-triene (95891-62-6) + (C6H4(PC6H5)3)(Fe(CO)4)2 (57139-05-6) + (C6H4(PC6H5)2)Fe2(CO)6 + (C6H4(PC6H5)3)Fe3(CO)9

Guidance literature:

In benzene; under N2 or Ar, Fe-compd. added in one portion to soln. of P-compd. at 70°C, refluxed for 0.5 h, various yields for various conditions; cooled, chromy. on silica gel with hexane/ethyl acetate, concd., preparative HPLC on silica gel with hexane/ethyl acetate, recrystd., elem. anal.;

Reference yield:

triiron dodecarbonyl (17685-52-8) + 1,2,3-triphenyl-1,2,3-triphosphaindane (89104-79-0,57194-41-9,5994-68-3) → [4,4,4,5,5,5-hexacarbonyl-2,3,6-triphenyl-2,3,6-triphospha-4,5-diferratetracyclo[5.4.0.0(3,5).0(4,6).]undeca7(1),8,10-triene]tetracarbonyliron (89210-02-6) + 3,3,3,4,4,4,6,6,6-nonacarbonyl-2,5,7-triphenyl-2,5,7-triphospha-3,4,6-triferrapentacyclo[6.4.0.0(2,6).0(3,5).0(4,7).]dodeca-8(1),9,11-triene (95891-62-6) + (C6H4(PC6H5)3)(Fe(CO)4)2 (57139-05-6) + (C6H4(PC6H5)2)Fe2(CO)6 + (C6H4(PC6H5)3)Fe3(CO)9

Guidance literature:

In benzene; under N2 or Ar, soln. of P-compd. and Fe-compd. refluxed for about 15 min; HPLC;

Reference yield: 100.0%

[4,4,4,5,5,5-hexacarbonyl-2,3,6-triphenyl-2,3,6-triphospha-4,5-diferratetracyclo[5.4.0.0(3,5).0(4,6).]undeca7(1),8,10-triene]tetracarbonyliron (89210-02-6) → (C6H4(PC6H5)3)Fe3(CO)9

Guidance literature:

In benzene; under N2 or Ar, treated at 80.5°C for 11.5 min, various yields for various reaction times; HPLC; Kinetics;

upstream raw materials:

triiron dodecarbonyl

1,2,3-triphenyl-1,2,3-triphosphaindane

diiron nonacarbonyl

Downstream raw materials:

3,3,3,4,4,4,6,6,6-nonacarbonyl-2,5,7-triphenyl-2,5,7-triphospha-3,4,6-triferrapentacyclo[6.4.0.0(2,6).0(3,5).0(4,7).]dodeca-8⁽¹⁾,9,11-triene

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