1,8,17,24-tetraoxa<8.8>(2,6)-naphthalenophane-3,5,19,21-tetrayne-10,30-dicarboxylic acid bis(3-phenylpropyl) ester

Base Information

Chemical Name:1,8,17,24-tetraoxa<8.8>(2,6)-naphthalenophane-3,5,19,21-tetrayne-10,30-dicarboxylic acid bis(3-phenylpropyl) ester
CAS No.:83487-58-5
Molecular Formula:C₅₂H₄₀O₈
Molecular Weight:792.885
Hs Code.:

Synonyms:1,8,17,24-tetraoxa<8.8>(2,6)-naphthalenophane-3,5,19,21-tetrayne-10,30-dicarboxylic acid bis(3-phenylpropyl) ester

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Chemical Property of 1,8,17,24-tetraoxa<8.8>(2,6)-naphthalenophane-3,5,19,21-tetrayne-10,30-dicarboxylic acid bis(3-phenylpropyl) ester

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Technology Process of 1,8,17,24-tetraoxa<8.8>(2,6)-naphthalenophane-3,5,19,21-tetrayne-10,30-dicarboxylic acid bis(3-phenylpropyl) ester

There total 8 articles about 1,8,17,24-tetraoxa<8.8>(2,6)-naphthalenophane-3,5,19,21-tetrayne-10,30-dicarboxylic acid bis(3-phenylpropyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 83487-57-4
C₅₂H₄₂O₈

: 83487-58-5
1,8,17,24-tetraoxa<8.8>(2,6)-naphthalenophane-3,5,19,21-tetrayne-10,30-dicarboxylic acid bis(3-phenylpropyl) ester

Guidance literature:: With copper diacetate; In pyridine; at 44 ℃; for 4h;
DOI:10.1021/ja00389a050

Reference yield:

: 637-59-2
1-Bromo-3-phenylpropane

: 83487-58-5
1,8,17,24-tetraoxa<8.8>(2,6)-naphthalenophane-3,5,19,21-tetrayne-10,30-dicarboxylic acid bis(3-phenylpropyl) ester

Guidance literature:: Multi-step reaction with 5 steps

1: 12 h / 90 °C

2: K₂CO₃ / acetone / Heating

3: cupric acetate monohydrate / pyridine / 45 °C

4: K₂CO₃ / acetone / Heating

5: 50 percent / cupric acetate monohydrate / pyridine / 4 h / 44 °C

With copper diacetate; potassium carbonate; In pyridine; acetone;
DOI:10.1021/ja00389a050

Reference yield:

: 83511-07-3
3,7-dihydroxy-2-naphthoic acid

: 83487-58-5
1,8,17,24-tetraoxa<8.8>(2,6)-naphthalenophane-3,5,19,21-tetrayne-10,30-dicarboxylic acid bis(3-phenylpropyl) ester

Guidance literature:: Multi-step reaction with 5 steps

1: 12 h / 90 °C

2: K₂CO₃ / acetone / Heating

3: cupric acetate monohydrate / pyridine / 45 °C

4: K₂CO₃ / acetone / Heating

5: 50 percent / cupric acetate monohydrate / pyridine / 4 h / 44 °C

With copper diacetate; potassium carbonate; In pyridine; acetone;
DOI:10.1021/ja00389a050