carbonic acid 4-bromomethyl-2-tert-butoxycarbonyloxyphenyl ester tert-butyl ester

Base Information

• Chemical Name: carbonic acid 4-bromomethyl-2-tert-butoxycarbonyloxyphenyl ester tert-butyl ester
• CAS No.: 1036243-96-5
• Molecular Formula: C₁₇H₂₃BrO₆
• Molecular Weight: 403.27

Synonyms:carbonic acid 4-bromomethyl-2-tert-butoxycarbonyloxyphenyl ester tert-butyl ester

Chemical Property of carbonic acid 4-bromomethyl-2-tert-butoxycarbonyloxyphenyl ester tert-butyl ester

Chemical Property:

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Technology Process of carbonic acid 4-bromomethyl-2-tert-butoxycarbonyloxyphenyl ester tert-butyl ester

There total 1 articles about carbonic acid 4-bromomethyl-2-tert-butoxycarbonyloxyphenyl ester tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

carbonic acid 2-tert-butoxycarbonyloxy-4-hydroxymethylphenyl ester tert-butyl ester (1036243-94-3) → carbonic acid 4-bromomethyl-2-tert-butoxycarbonyloxyphenyl ester tert-butyl ester (1036243-96-5)

Guidance literature:

With phosphorus tribromide; In dichloromethane; at 0 ℃; for 1h;

DOI:10.1016/j.tet.2008.02.108

Reference yield: 62.0%

carbonic acid 4-bromomethyl-2-tert-butoxycarbonyloxyphenyl ester tert-butyl ester (1036243-96-5) + triphenylphosphine (603-35-0) → [3,4-bis(tert-tert-butoxycarbonyloxy)-benzyl]-triphenylphosphonium bromide (1036243-58-9)

Guidance literature:

In toluene; at 60 ℃;

DOI:10.1016/j.tet.2008.02.108

upstream raw materials:

carbonic acid 2-tert-butoxycarbonyloxy-4-hydroxymethylphenyl ester tert-butyl ester

Downstream raw materials:

[3,4-bis(tert-tert-butoxycarbonyloxy)-benzyl]-triphenylphosphonium bromide

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