[3,4-bis(tert-tert-butoxycarbonyloxy)-benzyl]-triphenylphosphonium bromide

Base Information

Chemical Name:[3,4-bis(tert-tert-butoxycarbonyloxy)-benzyl]-triphenylphosphonium bromide
CAS No.:1036243-58-9
Molecular Formula:Br*C₃₅H₃₈O₆P
Molecular Weight:665.561
Hs Code.:

Synonyms:[3,4-bis(tert-tert-butoxycarbonyloxy)-benzyl]-triphenylphosphonium bromide

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Chemical Property of [3,4-bis(tert-tert-butoxycarbonyloxy)-benzyl]-triphenylphosphonium bromide

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Technology Process of [3,4-bis(tert-tert-butoxycarbonyloxy)-benzyl]-triphenylphosphonium bromide

There total 1 articles about [3,4-bis(tert-tert-butoxycarbonyloxy)-benzyl]-triphenylphosphonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1036243-96-5
carbonic acid 4-bromomethyl-2-tert-butoxycarbonyloxyphenyl ester tert-butyl ester

: 603-35-0
triphenylphosphine

: 1036243-58-9
[3,4-bis(tert-tert-butoxycarbonyloxy)-benzyl]-triphenylphosphonium bromide

Guidance literature:: In toluene; at 60 ℃;
DOI:10.1016/j.tet.2008.02.108

Reference yield: 46.0%

: 959588-81-9
[4-bromo-3,5-bis-(1,1-dimethyl-allyloxy)]benzaldehyde

: 1036243-58-9
[3,4-bis(tert-tert-butoxycarbonyloxy)-benzyl]-triphenylphosphonium bromide

: 959588-78-4
(E)-carbonic acid 4-{2-[4-bromo-3,5-bis(1,1-dimethylallyloxy)phenyl]-vinyl}-2-tert-butoxycarbonyloxy-phenyl ester tert-butyl ester

: 1036244-43-5
(Z)-carbonic acid 4-{2-[4-bromo-3,5-bis(1,1-dimethylallyloxy)phenyl]-vinyl}-2-tert-butoxycarbonyloxy-phenyl ester tert-butyl ester

Guidance literature:: [3,4-bis(tert-tert-butoxycarbonyloxy)-benzyl]-triphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

[4-bromo-3,5-bis-(1,1-dimethyl-allyloxy)]benzaldehyde; In tetrahydrofuran; hexane; at -78 - 23 ℃; for 0.5h; Further stages.;
DOI:10.1016/j.tet.2008.02.108