(S)-2-((S)-6-Benzyloxycarbonylamino-2-hexadecanoylamino-hexanoylamino)-succinic acid dimethyl ester

Base Information

Chemical Name:(S)-2-((S)-6-Benzyloxycarbonylamino-2-hexadecanoylamino-hexanoylamino)-succinic acid dimethyl ester
CAS No.:115446-35-0
Molecular Formula:C₃₆H₅₉N₃O₈
Molecular Weight:661.88
Hs Code.:

Synonyms:(S)-2-((S)-6-Benzyloxycarbonylamino-2-hexadecanoylamino-hexanoylamino)-succinic acid dimethyl ester

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Chemical Property of (S)-2-((S)-6-Benzyloxycarbonylamino-2-hexadecanoylamino-hexanoylamino)-succinic acid dimethyl ester

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Technology Process of (S)-2-((S)-6-Benzyloxycarbonylamino-2-hexadecanoylamino-hexanoylamino)-succinic acid dimethyl ester

There total 3 articles about (S)-2-((S)-6-Benzyloxycarbonylamino-2-hexadecanoylamino-hexanoylamino)-succinic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.6%

: 6384-18-5
L-Aspartic acid dimethyl ester

: (S)-2-Hexadecanoylamino-6-(2-phenoxy-acetylamino)-hexanoic acid

: 115446-35-0
(S)-2-((S)-6-Benzyloxycarbonylamino-2-hexadecanoylamino-hexanoylamino)-succinic acid dimethyl ester

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In ethyl acetate; at 5 ℃; for 72h;
DOI:10.1271/bbb1961.52.765

Reference yield:

: (S)-2-Amino-6-(2-phenoxy-acetylamino)-hexanoic acid

: 115446-35-0
(S)-2-((S)-6-Benzyloxycarbonylamino-2-hexadecanoylamino-hexanoylamino)-succinic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 63.2 percent / NaOH / H₂O; dioxane / 2 h / 0 °C

2: 42.6 percent / N-hydroxybenzotriazole, DCC / ethyl acetate / 72 h / 5 °C

With sodium hydroxide; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In 1,4-dioxane; water; ethyl acetate;
DOI:10.1271/bbb1961.52.765

Reference yield:

: 112-67-4
n-hexadecanoyl chloride

: 115446-35-0
(S)-2-((S)-6-Benzyloxycarbonylamino-2-hexadecanoylamino-hexanoylamino)-succinic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 63.2 percent / NaOH / H₂O; dioxane / 2 h / 0 °C

2: 42.6 percent / N-hydroxybenzotriazole, DCC / ethyl acetate / 72 h / 5 °C

With sodium hydroxide; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In 1,4-dioxane; water; ethyl acetate;
DOI:10.1271/bbb1961.52.765