2-acetoxy-3-(4-((2,3,4-trimethoxyphenyl)methyl)-piperazine-1-yl)propane-1-sulfonic acid sodium salt

Base Information

Chemical Name:2-acetoxy-3-(4-((2,3,4-trimethoxyphenyl)methyl)-piperazine-1-yl)propane-1-sulfonic acid sodium salt
CAS No.:1383744-23-7
Molecular Formula:C₁₉H₂₉N₂O₈S*Na
Molecular Weight:468.504
Hs Code.:

Synonyms:2-acetoxy-3-(4-((2,3,4-trimethoxyphenyl)methyl)-piperazine-1-yl)propane-1-sulfonic acid sodium salt

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Chemical Property of 2-acetoxy-3-(4-((2,3,4-trimethoxyphenyl)methyl)-piperazine-1-yl)propane-1-sulfonic acid sodium salt

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Technology Process of 2-acetoxy-3-(4-((2,3,4-trimethoxyphenyl)methyl)-piperazine-1-yl)propane-1-sulfonic acid sodium salt

There total 2 articles about 2-acetoxy-3-(4-((2,3,4-trimethoxyphenyl)methyl)-piperazine-1-yl)propane-1-sulfonic acid sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 506-96-7
Acetyl bromide

: 1383744-11-3
3-(1-(2,3,4-trimethoxybenzyl)piperazine-4-yl)-2-hydroxy-1-propanesulfonic acid sodium salt

: 1383744-23-7
2-acetoxy-3-(4-((2,3,4-trimethoxyphenyl)methyl)-piperazine-1-yl)propane-1-sulfonic acid sodium salt

Guidance literature:: With triethylamine; In dichloromethane; at 10 - 20 ℃; Cooling with ice;

Reference yield:

: 13171-25-0,127881-54-3
trimetazidine dihydrochloride

: 1383744-23-7
2-acetoxy-3-(4-((2,3,4-trimethoxyphenyl)methyl)-piperazine-1-yl)propane-1-sulfonic acid sodium salt

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydrogencarbonate / water

1.2: 5 h / pH 9 / Reflux

2.1: triethylamine / dichloromethane / 10 - 20 °C / Cooling with ice

With sodium hydrogencarbonate; triethylamine; In dichloromethane; water;