Methyl 2-{[3-(2-Bromoethoxy)-2-phenylquinolin-4-yl]carbonyl}-1-phenylhydrazinecarboxylate

Base Information

Chemical Name:Methyl 2-{[3-(2-Bromoethoxy)-2-phenylquinolin-4-yl]carbonyl}-1-phenylhydrazinecarboxylate
CAS No.:914656-05-6
Molecular Formula:C₂₆H₂₂BrN₃O₄
Molecular Weight:520.382
Hs Code.:

Synonyms:Methyl 2-{[3-(2-Bromoethoxy)-2-phenylquinolin-4-yl]carbonyl}-1-phenylhydrazinecarboxylate

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Chemical Property of Methyl 2-{[3-(2-Bromoethoxy)-2-phenylquinolin-4-yl]carbonyl}-1-phenylhydrazinecarboxylate

Chemical Property:

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Technology Process of Methyl 2-{[3-(2-Bromoethoxy)-2-phenylquinolin-4-yl]carbonyl}-1-phenylhydrazinecarboxylate

There total 3 articles about Methyl 2-{[3-(2-Bromoethoxy)-2-phenylquinolin-4-yl]carbonyl}-1-phenylhydrazinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 914656-00-1
methyl 2-{[3-(2-hydroxyethoxy)-2-phenylquinolin-4-yl]carbonyl}-1-phenylhydrazinecarboxylate

: 914656-05-6
Methyl 2-{[3-(2-Bromoethoxy)-2-phenylquinolin-4-yl]carbonyl}-1-phenylhydrazinecarboxylate

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In dichloromethane;
DOI:10.1016/j.bmcl.2006.08.085

Reference yield:

: 875754-99-7
3-hydroxy-2-phenyl-4-quinolinecarboxylic acid, 2-(methoxycarbonyl)-2-phenylhydrazide

: 914656-05-6
Methyl 2-{[3-(2-Bromoethoxy)-2-phenylquinolin-4-yl]carbonyl}-1-phenylhydrazinecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: NaI; K₂CO₃ / tetrahydrofuran

2: LiBH₄ / tetrahydrofuran

3: CBr₄; Ph₃P / CH₂Cl₂

With lithium borohydride; carbon tetrabromide; potassium carbonate; triphenylphosphine; sodium iodide; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2006.08.085

Reference yield:

: 914654-35-6
methyl 2-{[3-(2-methoxy-2-oxoethoxy)-2-phenylquinolin-4-yl]carbonyl}-1-phenylhydrazinecarboxylate

: 914656-05-6
Methyl 2-{[3-(2-Bromoethoxy)-2-phenylquinolin-4-yl]carbonyl}-1-phenylhydrazinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: LiBH₄ / tetrahydrofuran

2: CBr₄; Ph₃P / CH₂Cl₂

With lithium borohydride; carbon tetrabromide; triphenylphosphine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2006.08.085