tert-butyl (1R,3R)-2-hydroxy-1,3-bis(4-methoxyphenyl)propane-1,3-diyldicarbamate

Base Information

Chemical Name:tert-butyl (1R,3R)-2-hydroxy-1,3-bis(4-methoxyphenyl)propane-1,3-diyldicarbamate
CAS No.:1374758-62-9
Molecular Formula:C₂₇H₃₈N₂O₇
Molecular Weight:502.608
Hs Code.:

Synonyms:tert-butyl (1R,3R)-2-hydroxy-1,3-bis(4-methoxyphenyl)propane-1,3-diyldicarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl (1R,3R)-2-hydroxy-1,3-bis(4-methoxyphenyl)propane-1,3-diyldicarbamate

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Technology Process of tert-butyl (1R,3R)-2-hydroxy-1,3-bis(4-methoxyphenyl)propane-1,3-diyldicarbamate

There total 2 articles about tert-butyl (1R,3R)-2-hydroxy-1,3-bis(4-methoxyphenyl)propane-1,3-diyldicarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1374758-59-4
tert-butyl (1R,3R)-1,3-bis(4-methoxyphenyl)-2-oxopropane-1,3-diyldicarbamate

: 1374758-62-9
tert-butyl (1R,3R)-2-hydroxy-1,3-bis(4-methoxyphenyl)propane-1,3-diyldicarbamate

Guidance literature:: With sodium tetrahydroborate; In methanol; for 0.5h;
DOI:10.1002/anie.201107473

Reference yield:

: 1152166-56-7
tert-butyl-(1S,3S)-2-formyl-1,3-bis(4-methoxyphenyl)propane-1,3-diyldicarbamate

: 1374758-62-9
tert-butyl (1R,3R)-2-hydroxy-1,3-bis(4-methoxyphenyl)propane-1,3-diyldicarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: oxygen; 4-methoxy-aniline / toluene / 37 h / 20 - 50 °C / 7600.51 Torr

2: sodium tetrahydroborate / methanol / 0.5 h

With sodium tetrahydroborate; oxygen; 4-methoxy-aniline; In methanol; toluene;
DOI:10.1002/anie.201107473