N⁶-benzoyl-3'-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine 2'-<2,5-dichlorophenyl 2-(4-nitrophenyl)ethyl phosphate>

Base Information

• Chemical Name: N⁶-benzoyl-3'-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine 2'-<2,5-dichlorophenyl 2-(4-nitrophenyl)ethyl phosphate>
• CAS No.: 80727-10-2
• Molecular Formula: C₅₇H₅₇Cl₂N₆O₁₁PSi
• Molecular Weight: 1132.08

Synonyms:N⁶-benzoyl-3'-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine 2'-<2,5-dichlorophenyl 2-(4-nitrophenyl)ethyl phosphate>

Chemical Property of N⁶-benzoyl-3'-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine 2'-<2,5-dichlorophenyl 2-(4-nitrophenyl)ethyl phosphate>

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Technology Process of N⁶-benzoyl-3'-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine 2'-<2,5-dichlorophenyl 2-(4-nitrophenyl)ethyl phosphate>

There total 1 articles about N⁶-benzoyl-3'-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine 2'-<2,5-dichlorophenyl 2-(4-nitrophenyl)ethyl phosphate> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(4-nitrophenyl)ethanol (100-27-6) + 2,5-dichlorophenyl phosphorodichloridate (53676-18-9) + N6-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine (69504-10-5) → N6-benzoyl-3'-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine 2'-<2,5-dichlorophenyl 2-(4-nitrophenyl)ethyl phosphate> (80727-10-2)

Guidance literature:

Yield given. Multistep reaction;

Reference yield: 95.0%

N6-benzoyl-3'-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine 2'-<2,5-dichlorophenyl 2-(4-nitrophenyl)ethyl phosphate> (80727-10-2) + triethylamine (121-44-8) → Triethylammonium-6-benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenosin-2'-<2-(4-nitrophenyl)ethyl>phosphat> (80727-12-4)

Guidance literature:

With 4-nitrobenzaldehyde oxime; In 1,4-dioxane; water; for 2h; Ambient temperature;

Reference yield: 92.0%

N6-benzoyl-3'-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine 2'-<2,5-dichlorophenyl 2-(4-nitrophenyl)ethyl phosphate> (80727-10-2) → N6-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>adenosine 2'-<2,5-dichlorophenyl 2-(4-nitrophenyl)ethyl phosphate>

Guidance literature:

With toluene-4-sulfonic acid; In methanol; dichloromethane; for 0.5h;

DOI:10.1002/hlca.19890720811

upstream raw materials:

2-(4-nitrophenyl)ethanol

2,5-dichlorophenyl phosphorodichloridate

N⁶-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine

Downstream raw materials:

Triethylammonium-6-benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenosin-2'-<2-(4-nitrophenyl)ethyl>phosphat>

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