2,6-O-bis(benzyloxymethyl)-3,4,5-O-tris(dibenzylphosphoryl)-D-myo-inositol 1-O-(1,2-O-dipalmitoyl)-sn-glyceryl 2-cyanoethyl phosphate

Base Information

Chemical Name:2,6-O-bis(benzyloxymethyl)-3,4,5-O-tris(dibenzylphosphoryl)-D-myo-inositol 1-O-(1,2-O-dipalmitoyl)-sn-glyceryl 2-cyanoethyl phosphate
CAS No.:183429-91-6
Molecular Formula:C₁₀₂H₁₃₇NO₂₄P₄
Molecular Weight:1885.1
Hs Code.:

Synonyms:2,6-O-bis(benzyloxymethyl)-3,4,5-O-tris(dibenzylphosphoryl)-D-myo-inositol 1-O-(1,2-O-dipalmitoyl)-sn-glyceryl 2-cyanoethyl phosphate

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Chemical Property of 2,6-O-bis(benzyloxymethyl)-3,4,5-O-tris(dibenzylphosphoryl)-D-myo-inositol 1-O-(1,2-O-dipalmitoyl)-sn-glyceryl 2-cyanoethyl phosphate

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Technology Process of 2,6-O-bis(benzyloxymethyl)-3,4,5-O-tris(dibenzylphosphoryl)-D-myo-inositol 1-O-(1,2-O-dipalmitoyl)-sn-glyceryl 2-cyanoethyl phosphate

There total 1 articles about 2,6-O-bis(benzyloxymethyl)-3,4,5-O-tris(dibenzylphosphoryl)-D-myo-inositol 1-O-(1,2-O-dipalmitoyl)-sn-glyceryl 2-cyanoethyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108549-23-1
Dibenzyl N,N-diisopropylphosphoramidite

: 183429-89-2
Hexadecanoic acid (R)-2-[((1S,2R,3R,4S,5S,6R)-2,6-bis-benzyloxymethoxy-3,4,5-trihydroxy-cyclohexyloxy)-(2-cyano-ethoxy)-phosphoryloxy]-1-hexadecanoyloxymethyl-ethyl ester

: 183429-91-6
2,6-O-bis(benzyloxymethyl)-3,4,5-O-tris(dibenzylphosphoryl)-D-myo-inositol 1-O-(1,2-O-dipalmitoyl)-sn-glyceryl 2-cyanoethyl phosphate

Guidance literature:: With 1H-tetrazole; 3-chloro-benzenecarboperoxoic acid; Yield given. Multistep reaction; 1.) CH₂Cl₂, 24 deg C, 1 h, 2.) CH₂Cl₂, -40 deg C, 1 h;
DOI:10.1021/jo961226g

Reference yield: 97.0%

: 7087-68-5
N-ethyl-N,N-diisopropylamine

: 183429-91-6
2,6-O-bis(benzyloxymethyl)-3,4,5-O-tris(dibenzylphosphoryl)-D-myo-inositol 1-O-(1,2-O-dipalmitoyl)-sn-glyceryl 2-cyanoethyl phosphate

: 2,6-O-bis(benzyloxymethyl)-3,4,5-O-tris(dibenzylphosphoryl)-D-myo-inositol 1-O-(1,2-O-dipalmitoyl)-sn-glyceryl diisopropylethylammonium phosphate

Guidance literature:: In acetonitrile; at 60 ℃; for 12h;
DOI:10.1021/jo961226g

Reference yield: 80.0%

: 183429-91-6
2,6-O-bis(benzyloxymethyl)-3,4,5-O-tris(dibenzylphosphoryl)-D-myo-inositol 1-O-(1,2-O-dipalmitoyl)-sn-glyceryl 2-cyanoethyl phosphate

: 3,4,5-tri-O-phosphoryl-D-myo-inositol 1-O-(1,2-O-dipalmitoyl)-sn-glyceryl 3-aminopropyl phosphate sodium salt

Guidance literature:: With hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In water; tert-butyl alcohol; for 21h; under 2637.5 Torr;
DOI:10.1021/jo961226g