2-hydroxymethylene-4-{[2-(4-phenylpiperazin-1-yl)ethyl]propylamino}cyclohexanone

Base Information

Chemical Name:2-hydroxymethylene-4-{[2-(4-phenylpiperazin-1-yl)ethyl]propylamino}cyclohexanone
CAS No.:1026083-45-3
Molecular Formula:C₂₂H₃₃N₃O₂
Molecular Weight:371.523
Hs Code.:

Synonyms:2-hydroxymethylene-4-{[2-(4-phenylpiperazin-1-yl)ethyl]propylamino}cyclohexanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-hydroxymethylene-4-{[2-(4-phenylpiperazin-1-yl)ethyl]propylamino}cyclohexanone

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Technology Process of 2-hydroxymethylene-4-{[2-(4-phenylpiperazin-1-yl)ethyl]propylamino}cyclohexanone

There total 1 articles about 2-hydroxymethylene-4-{[2-(4-phenylpiperazin-1-yl)ethyl]propylamino}cyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 109-94-4
formic acid ethyl ester

: 477788-92-4
4-{[2-(4-phenyl-piperazin-1-yl)-ethyl]-propyl-amino}-cyclohexanone

: 1026083-45-3
2-hydroxymethylene-4-{[2-(4-phenylpiperazin-1-yl)ethyl]propylamino}cyclohexanone

Guidance literature:: 4-{[2-(4-phenyl-piperazin-1-yl)-ethyl]-propyl-amino}-cyclohexanone; With sodium ethanolate; In benzene; at 0 ℃; for 0.166667h; Inert atmosphere;

formic acid ethyl ester; In benzene; at 20 ℃; Inert atmosphere;

With hydrogenchloride; In water;
DOI:10.1021/jm701524h

Reference yield: 80.0%

: 1026083-45-3
2-hydroxymethylene-4-{[2-(4-phenylpiperazin-1-yl)ethyl]propylamino}cyclohexanone

: 874459-30-0
[2-(4-phenylpiperazin-1-yl)ethyl]propyl(4,5,6,7-tetrahydrobenzo[d]isoxazol-5-yl)amine

Guidance literature:: With hydroxylamine hydrochloride; acetic acid; at 80 ℃; for 1h;
DOI:10.1021/jm701524h

Reference yield: 69.0%

: 1026083-45-3
2-hydroxymethylene-4-{[2-(4-phenylpiperazin-1-yl)ethyl]propylamino}cyclohexanone

: 874459-31-1
N-(2-(4-phenylpiperazin-1-yl)ethyl)-N-propyl-4,5,6,7-tetrahydro-1H-indazol-5-amine

Guidance literature:: 2-hydroxymethylene-4-{[2-(4-phenylpiperazin-1-yl)ethyl]propylamino}cyclohexanone; With semicarbazide hydrochloride; sodium acetate; In ethanol; water; at 0 ℃; for 1h;

With sulfuric acid; water; for 0.25h; Reflux;
DOI:10.1021/jm701524h