5-chloro-1-[(2,4-dimethoxyphenyl)sulphonyl]-3-(2-methoxyphenyl)-2-oxo-2,3-dihydro-1H-indol-3-yl phenyl carbamate

Base Information

• Chemical Name: 5-chloro-1-[(2,4-dimethoxyphenyl)sulphonyl]-3-(2-methoxyphenyl)-2-oxo-2,3-dihydro-1H-indol-3-yl phenyl carbamate
• CAS No.: 492430-48-5
• Molecular Formula: C₃₀H₂₅ClN₂O₈S
• Molecular Weight: 609.056

Synonyms:5-chloro-1-[(2,4-dimethoxyphenyl)sulphonyl]-3-(2-methoxyphenyl)-2-oxo-2,3-dihydro-1H-indol-3-yl phenyl carbamate

Chemical Property of 5-chloro-1-[(2,4-dimethoxyphenyl)sulphonyl]-3-(2-methoxyphenyl)-2-oxo-2,3-dihydro-1H-indol-3-yl phenyl carbamate

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Technology Process of 5-chloro-1-[(2,4-dimethoxyphenyl)sulphonyl]-3-(2-methoxyphenyl)-2-oxo-2,3-dihydro-1H-indol-3-yl phenyl carbamate

There total 1 articles about 5-chloro-1-[(2,4-dimethoxyphenyl)sulphonyl]-3-(2-methoxyphenyl)-2-oxo-2,3-dihydro-1H-indol-3-yl phenyl carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-amino-5-chloro-1-[(2,4-dimethoxy-phenyl)sulphonyl]-3-(2-methoxyphenyl)-1,3-dihydro-1H-indol-2-one (492430-49-6,492430-53-2) + phenyl chloroformate (1885-14-9) → 5-chloro-1-[(2,4-dimethoxyphenyl)sulphonyl]-3-(2-methoxyphenyl)-2-oxo-2,3-dihydro-1H-indol-3-yl phenyl carbamate (492430-48-5)

Guidance literature:

With pyridine; In dichloromethane; at 4 - 20 ℃; for 1h;

Reference yield:

5-chloro-1-[(2,4-dimethoxyphenyl)sulphonyl]-3-(2-methoxyphenyl)-2-oxo-2,3-dihydro-1H-indol-3-yl phenyl carbamate (492430-48-5) + 1-(2-pyridinyl)-1,4-diazepane (287114-32-3) → N-[5-chloro-1-[(2,4-dimethoxyphenyl)-sulphonyl]-3-(2-methoxyphenyl)-2-oxo-2,3-dihydro-1H-indol-3-yl]-4-(2-pyridyl)homopiperazine-1-carboxamide

Guidance literature:

In dichloromethane; at 20 ℃; for 18h;

Reference yield:

5-chloro-1-[(2,4-dimethoxyphenyl)sulphonyl]-3-(2-methoxyphenyl)-2-oxo-2,3-dihydro-1H-indol-3-yl phenyl carbamate (492430-48-5) + 4-(piperazin-1-yl)pyridine (1008-91-9) → N-[5-chloro-1-[(2,4-dimethoxyphenyl)-sulphonyl]-3-(2-methoxyphenyl)-2-oxo-2,3-dihydro-1H-indol-3-yl]-4-(4-pyridyl)piperazine-1-carboxamide

Guidance literature:

In chloroform; for 4h; Heating / reflux;

upstream raw materials:

3-amino-5-chloro-1-[(2,4-dimethoxy-phenyl)sulphonyl]-3-(2-methoxyphenyl)-1,3-dihydro-1H-indol-2-one

phenyl chloroformate

Downstream raw materials:

N-[5-chloro-1-[(2,4-dimethoxyphenyl)-sulphonyl]-3-(2-methoxyphenyl)-2-oxo-2,3-dihydro-1H-indol-3-yl]-4-(4-pyridyl)homopiperazine-1-carboxamide

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