chlorobis-{(R)-1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C2,N}{μ-{2-(diphenylphosphino)ethanethiolato-P,S:S}}dipalladium (II)

Base Information

Chemical Name:chlorobis-{(R)-1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C2,N}{μ-{2-(diphenylphosphino)ethanethiolato-P,S:S}}dipalladium (II)
CAS No.:139276-71-4
Molecular Formula:0CH₂Cl₂*C₄₂H₄₆ClN₂PPd₂S
Molecular Weight:932.64
Hs Code.:

Synonyms:chlorobis-{(R)-1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C2,N}{μ-{2-(diphenylphosphino)ethanethiolato-P,S:S}}dipalladium (II)

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Chemical Property of chlorobis-{(R)-1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C2,N}{μ-{2-(diphenylphosphino)ethanethiolato-P,S:S}}dipalladium (II)

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Technology Process of chlorobis-{(R)-1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C2,N}{μ-{2-(diphenylphosphino)ethanethiolato-P,S:S}}dipalladium (II)

There total 1 articles about chlorobis-{(R)-1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C2,N}{μ-{2-(diphenylphosphino)ethanethiolato-P,S:S}}dipalladium (II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 80145-77-3
bis(μ-chloro){bis{(R)-1-(dimethylamino)ethyl}naphthylenyl-C2,N}-dipalladium(II) dichloromethane

: 3190-79-2
(2-mercaptoethyl)diphenylphosphine

: 139276-71-4
chlorobis-{(R)-1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C2,N}{μ-{2-(diphenylphosphino)ethanethiolato-P,S:S}}dipalladium (II)

Guidance literature:: With triethylamine; In dichloromethane; byproducts: Et3NHCl; stirred until the soln. was homogeneous; washed (water); org. layer sepd.; dried (MgSO4); solvent removed; crystd (dichloromethane/methanole); elem. anal.;

Reference yield: 86.0%

: 139276-71-4
chlorobis-{(R)-1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C2,N}{μ-{2-(diphenylphosphino)ethanethiolato-P,S:S}}dipalladium (II)

: 139276-72-5
{(R)-1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C₂,N}{2-(diphenylphosphino)ethanethiolato-P,S} palladium (II)

Guidance literature:: With diamino-1,2-ethane; In dichloromethane; water; (N2), stirred (10 min); excess ethylenediamine (water); org. phase sepd.; washed (water); dried (MgSO4); solvent removed; elem. anal.;