C₃₄H₄₇NO₅Si₂

Base Information

Chemical Name:C₃₄H₄₇NO₅Si₂
CAS No.:1258864-08-2
Molecular Formula:C₃₄H₄₇NO₅Si₂
Molecular Weight:605.922
Hs Code.:

C<sub>34</sub>H<sub>47</sub>NO<sub>5</sub>Si<sub>2</sub>

Synonyms:C₃₄H₄₇NO₅Si₂

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Chemical Property of C₃₄H₄₇NO₅Si₂

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Technology Process of C₃₄H₄₇NO₅Si₂

There total 17 articles about C₃₄H₄₇NO₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1258864-07-1
C₃₄H₅₁NO₅Si₂

: 1258864-08-2
C₃₄H₄₇NO₅Si₂

Guidance literature:: With [bis(acetoxy)iodo]benzene; 2-azaadamantane-N-oxyl; In dichloromethane; at 20 ℃; for 4h;
DOI:10.3987/COM-10-12042

Reference yield:

: 1258863-99-8
C₁₆H₂₀ClNO₃

: 1258864-08-2
C₃₄H₄₇NO₅Si₂

Guidance literature:: Multi-step reaction with 19 steps

1.1: 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene / water; acetonitrile / 15 h / 0 °C

2.1: methanol / diethyl ether / 0 °C

3.1: toluene-4-sulfonic acid / toluene / 12 h / Reflux

4.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C

4.2: 0.25 h

5.1: sodium tetrahydroborate / methanol / 2 h / -40 °C

6.1: pyridinium p-toluenesulfonate / dichloromethane / 3 h / Reflux

7.1: diisobutylaluminium hydride / tetrahydrofuran / 9 h / -5 °C

8.1: dmap; triethylamine / dichloromethane / 3 h / Reflux

9.1: dimethylaluminum chloride / hexane; dichloromethane / 0.5 h / 0 - 20 °C

10.1: 1-methyl-2-azaadamantane-N-oxyl; [bis(acetoxy)iodo]benzene / dichloromethane / 12 h / 20 °C

11.1: Wilkinson's catalyst; diethylzinc / tetrahydrofuran / 3 h / -20 °C

12.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 12 h / 0 °C

13.1: sodium cyanoborohydride; acetic acid / tetrahydrofuran / 144 h / 0 °C

14.1: hydrogenchloride / 2,2,2-trifluoroethanol; water / 0.5 h / 20 °C

15.1: dmap; triethylamine / dichloromethane / 12 h / 20 °C

16.1: methanol / 2.5 h / 20 °C

17.1: dmap; triethylamine / dichloromethane / 12 h / 20 °C

18.1: silica gel / chloroform; ethyl acetate / 0.25 h

19.1: 2-azaadamantane-N-oxyl; [bis(acetoxy)iodo]benzene / dichloromethane / 4 h / 20 °C

With hydrogenchloride; methanol; dmap; 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium tetrahydroborate; Wilkinson's catalyst; 1-methyl-2-azaadamantane-N-oxyl; [bis(acetoxy)iodo]benzene; 2-azaadamantane-N-oxyl; diethylzinc; dimethylaluminum chloride; pyridinium p-toluenesulfonate; silica gel; diisobutylaluminium hydride; sodium cyanoborohydride; toluene-4-sulfonic acid; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; chloroform; 2,2,2-trifluoroethanol; water; ethyl acetate; toluene; acetonitrile; 4.1: Claisen condensation / 4.2: Claisen condensation / 11.1: Reformatsky reaction;
DOI:10.3987/COM-10-12042

Reference yield:

: 1258864-02-6
C₁₉H₂₀ClNO₄

: 1258864-08-2
C₃₄H₄₇NO₅Si₂

Guidance literature:: Multi-step reaction with 15 steps

1: sodium tetrahydroborate / methanol / 2 h / -40 °C

2: pyridinium p-toluenesulfonate / dichloromethane / 3 h / Reflux

3: diisobutylaluminium hydride / tetrahydrofuran / 9 h / -5 °C

4: dmap; triethylamine / dichloromethane / 3 h / Reflux

5: dimethylaluminum chloride / hexane; dichloromethane / 0.5 h / 0 - 20 °C

6: 1-methyl-2-azaadamantane-N-oxyl; [bis(acetoxy)iodo]benzene / dichloromethane / 12 h / 20 °C

7: Wilkinson's catalyst; diethylzinc / tetrahydrofuran / 3 h / -20 °C

8: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 12 h / 0 °C

9: sodium cyanoborohydride; acetic acid / tetrahydrofuran / 144 h / 0 °C

10: hydrogenchloride / 2,2,2-trifluoroethanol; water / 0.5 h / 20 °C

11: dmap; triethylamine / dichloromethane / 12 h / 20 °C

12: methanol / 2.5 h / 20 °C

13: dmap; triethylamine / dichloromethane / 12 h / 20 °C

14: silica gel / chloroform; ethyl acetate / 0.25 h

15: 2-azaadamantane-N-oxyl; [bis(acetoxy)iodo]benzene / dichloromethane / 4 h / 20 °C

With hydrogenchloride; methanol; dmap; sodium tetrahydroborate; Wilkinson's catalyst; 1-methyl-2-azaadamantane-N-oxyl; [bis(acetoxy)iodo]benzene; 2-azaadamantane-N-oxyl; diethylzinc; dimethylaluminum chloride; pyridinium p-toluenesulfonate; silica gel; diisobutylaluminium hydride; sodium cyanoborohydride; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; methanol; hexane; dichloromethane; chloroform; 2,2,2-trifluoroethanol; water; ethyl acetate; 7: Reformatsky reaction;
DOI:10.3987/COM-10-12042