{3-[3,3-bis(methoxycarbonyl)-2-phenylpropyl]phenyl}methyl methyl carbonate

Base Information

Chemical Name:{3-[3,3-bis(methoxycarbonyl)-2-phenylpropyl]phenyl}methyl methyl carbonate
CAS No.:1350906-59-0
Molecular Formula:C₂₂H₂₄O₇
Molecular Weight:400.428
Hs Code.:

Synonyms:{3-[3,3-bis(methoxycarbonyl)-2-phenylpropyl]phenyl}methyl methyl carbonate

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Chemical Property of {3-[3,3-bis(methoxycarbonyl)-2-phenylpropyl]phenyl}methyl methyl carbonate

Chemical Property:

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Technology Process of {3-[3,3-bis(methoxycarbonyl)-2-phenylpropyl]phenyl}methyl methyl carbonate

There total 5 articles about {3-[3,3-bis(methoxycarbonyl)-2-phenylpropyl]phenyl}methyl methyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 6626-84-2
dimethyl 2-benzylidenepropanedioate

: 1350906-46-5
methyl {3-[(trimethylsilyl)methyl]phenyl}methyl carbonate

: 1350906-59-0
{3-[3,3-bis(methoxycarbonyl)-2-phenylpropyl]phenyl}methyl methyl carbonate

Guidance literature:: With cesium fluoride; In N,N-dimethyl-formamide; at 60 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ol203089k

Reference yield:

: 620-20-2,130468-19-8
1-Chloro-3-chloromethyl-benzene

: 1350906-59-0
{3-[3,3-bis(methoxycarbonyl)-2-phenylpropyl]phenyl}methyl methyl carbonate

Guidance literature:: Multi-step reaction with 5 steps

1.1: magnesium / tetrahydrofuran / 4 h / 20 °C

2.1: iodine; lithium / tetrahydrofuran / 3.5 h / -40 °C / Inert atmosphere

2.2: 16 h / -40 - 20 °C / Inert atmosphere

3.1: sodium tetrahydroborate / methanol / 0.67 h / 0 °C

4.1: pyridine; dmap / dichloromethane / 4 h / 20 °C / Inert atmosphere

5.1: cesium fluoride / N,N-dimethyl-formamide / 3 h / 60 °C / Inert atmosphere

With pyridine; dmap; sodium tetrahydroborate; iodine; lithium; magnesium; cesium fluoride; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol203089k

Reference yield:

: 1350906-86-3
3-[(trimethylsilyl)methyl]benzaldehyde

: 1350906-59-0
{3-[3,3-bis(methoxycarbonyl)-2-phenylpropyl]phenyl}methyl methyl carbonate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / methanol / 0.67 h / 0 °C

2: pyridine; dmap / dichloromethane / 4 h / 20 °C / Inert atmosphere

3: cesium fluoride / N,N-dimethyl-formamide / 3 h / 60 °C / Inert atmosphere

With pyridine; dmap; sodium tetrahydroborate; cesium fluoride; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol203089k