3-(benzyloxymethyl)-2-[(1'S,2'S,4'S,5'R)-4'-hydroxy-5'-(hydroxymethyl)bicyclo[3.1.0]hexan-2'-yloxy]-5-methylpyrimidin-4(3H)-one

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Chemical Name:3-(benzyloxymethyl)-2-[(1'S,2'S,4'S,5'R)-4'-hydroxy-5'-(hydroxymethyl)bicyclo[3.1.0]hexan-2'-yloxy]-5-methylpyrimidin-4(3H)-one
CAS No.:1004771-20-3
Molecular Formula:C₂₀H₂₄N₂O₅
Molecular Weight:372.421
Hs Code.:

Synonyms:3-(benzyloxymethyl)-2-[(1'S,2'S,4'S,5'R)-4'-hydroxy-5'-(hydroxymethyl)bicyclo[3.1.0]hexan-2'-yloxy]-5-methylpyrimidin-4(3H)-one

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Chemical Property of 3-(benzyloxymethyl)-2-[(1'S,2'S,4'S,5'R)-4'-hydroxy-5'-(hydroxymethyl)bicyclo[3.1.0]hexan-2'-yloxy]-5-methylpyrimidin-4(3H)-one

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Technology Process of 3-(benzyloxymethyl)-2-[(1'S,2'S,4'S,5'R)-4'-hydroxy-5'-(hydroxymethyl)bicyclo[3.1.0]hexan-2'-yloxy]-5-methylpyrimidin-4(3H)-one

There total 1 articles about 3-(benzyloxymethyl)-2-[(1'S,2'S,4'S,5'R)-4'-hydroxy-5'-(hydroxymethyl)bicyclo[3.1.0]hexan-2'-yloxy]-5-methylpyrimidin-4(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 119451-90-0
3-((benzyloxy)methyl)-5-methylpyrimidine-2,4(1H,3H)-dione

: 452335-24-9
(1R,2S,4R,5S)-(2-acetoxy-4-hydroxybicyclo[3.1.0]hex-1-yl)methyl acetate

: 1004771-20-3
3-(benzyloxymethyl)-2-[(1'S,2'S,4'S,5'R)-4'-hydroxy-5'-(hydroxymethyl)bicyclo[3.1.0]hexan-2'-yloxy]-5-methylpyrimidin-4(3H)-one

: 1004771-19-0
3-(benzyloxymethyl)-1-[(1'S,2'S,4'S,5'R)-4'-hydroxy-5'-(hydroxymethyl)bicyclo[3.1.0]hexan-2'-yl]-5-methylpyrimidine-2,4(1H,3H)-dione

Guidance literature:: 3-((benzyloxy)methyl)-5-methylpyrimidine-2,4(1H,3H)-dione; (1R,2S,4R,5S)-(2-acetoxy-4-hydroxybicyclo[3.1.0]hex-1-yl)methyl acetate; With di-isopropyl azodicarboxylate; triphenylphosphine; In acetonitrile; at -40 - 20 ℃; for 15h;

In methanol; at 20 ℃; for 5h; Further stages.;
DOI:10.1055/s-2007-990847