N-phenylacetohydroxamic acid 2,3,4-tri-O-acetyl-β-D-glucopyranoside

Base Information

Chemical Name:N-phenylacetohydroxamic acid 2,3,4-tri-O-acetyl-β-D-glucopyranoside
CAS No.:1356933-21-5
Molecular Formula:C₂₀H₂₅NO₁₀
Molecular Weight:439.419
Hs Code.:

Synonyms:N-phenylacetohydroxamic acid 2,3,4-tri-O-acetyl-β-D-glucopyranoside

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Chemical Property of N-phenylacetohydroxamic acid 2,3,4-tri-O-acetyl-β-D-glucopyranoside

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Technology Process of N-phenylacetohydroxamic acid 2,3,4-tri-O-acetyl-β-D-glucopyranoside

There total 14 articles about N-phenylacetohydroxamic acid 2,3,4-tri-O-acetyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 108-24-7
acetic anhydride

: 98911-22-9
N-phenylacetohydroxamic acid β-D-glucopyranoside

: 1356933-21-5
N-phenylacetohydroxamic acid 2,3,4-tri-O-acetyl-β-D-glucopyranoside

Guidance literature:: N-phenylacetohydroxamic acid β-D-glucopyranoside; With pyridine; mono-4-methoxytrityl chloride; at 25 ℃; for 16h;

acetic anhydride; at 25 ℃; for 27h;

With acetic acid; In water; at 20 ℃; for 3h;
DOI:10.1021/jo202123s

Reference yield: 68.0%

: 1376932-95-4
C₂₁H₂₇NO₁₀

: 1356933-22-6
N-phenylacetohydroxamic acid 2,3,6-tri-O-acetyl-β-D-glucopyranoside

: 1356933-21-5
N-phenylacetohydroxamic acid 2,3,4-tri-O-acetyl-β-D-glucopyranoside

Guidance literature:: With acetic acid; In water; at 25 ℃; for 0.25h;
DOI:10.1021/jo202123s

Reference yield:

: 98911-14-9
N-phenylacetohydroxamic acid 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

: 1356933-21-5
N-phenylacetohydroxamic acid 2,3,4-tri-O-acetyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: Streptomyces rochei carboxylesterase; water / dimethyl sulfoxide / 2 h / 40 °C / pH 7.2 / aq. phosphate buffer; Enzymatic reaction

2.1: pyridine; mono-4-methoxytrityl chloride / 16 h / 25 °C

2.2: 27 h / 25 °C

2.3: 3 h / 20 °C

With pyridine; Streptomyces rochei carboxylesterase; water; mono-4-methoxytrityl chloride; In dimethyl sulfoxide;
DOI:10.1021/jo202123s