(2E,2'E)-dibutyl 3,3'-[2-(4-methoxyphenyl)-1-methyl-1H-imidazole-4,5-diyl]diacrylate

Base Information

• Chemical Name: (2E,2'E)-dibutyl 3,3'-[2-(4-methoxyphenyl)-1-methyl-1H-imidazole-4,5-diyl]diacrylate
• CAS No.: 1246624-50-9
• Molecular Formula: C₂₅H₃₂N₂O₅
• Molecular Weight: 440.539
• Mol file: 1246624-50-9.mol

Synonyms:(2E,2'E)-dibutyl 3,3'-[2-(4-methoxyphenyl)-1-methyl-1H-imidazole-4,5-diyl]diacrylate

Chemical Property of (2E,2'E)-dibutyl 3,3'-[2-(4-methoxyphenyl)-1-methyl-1H-imidazole-4,5-diyl]diacrylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (2E,2'E)-dibutyl 3,3'-[2-(4-methoxyphenyl)-1-methyl-1H-imidazole-4,5-diyl]diacrylate

There total 1 articles about (2E,2'E)-dibutyl 3,3'-[2-(4-methoxyphenyl)-1-methyl-1H-imidazole-4,5-diyl]diacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

acrylic acid n-butyl ester (141-32-2,9003-49-0) + 4,5-dibromo-1-methyl-2-(4-methoxyphenyl)imidazole (1246624-38-3) → (2E,2'E)-dibutyl 3,3'-[2-(4-methoxyphenyl)-1-methyl-1H-imidazole-4,5-diyl]diacrylate (1246624-50-9)

Guidance literature:

With palladium diacetate; triethylamine; tricyclohexylphosphine; In N,N-dimethyl-formamide; at 100 ℃; for 24h; Inert atmosphere; pressure tube;

DOI:10.1055/s-0030-1258092

Reference yield: 81.0%

(2E,2'E)-dibutyl 3,3'-[2-(4-methoxyphenyl)-1-methyl-1H-imidazole-4,5-diyl]diacrylate (1246624-50-9) → dibutyl 2-(4-methoxyphenyl)-1-methyl-1H-benzo[d]imidazole-5,6-dicarboxylate (1246624-98-5)

Guidance literature:

(2E,2'E)-dibutyl 3,3'-[2-(4-methoxyphenyl)-1-methyl-1H-imidazole-4,5-diyl]diacrylate; In diphenylether; at 200 ℃; for 24h; pressure tube;

With palladium 10% on activated carbon; In diphenylether; at 20 - 200 ℃; Inert atmosphere; pressure tube;

DOI:10.1055/s-0030-1258092

upstream raw materials:

acrylic acid n-butyl ester

4,5-dibromo-1-methyl-2-(4-methoxyphenyl)imidazole

Downstream raw materials:

dibutyl 2-(4-methoxyphenyl)-1-methyl-1H-benzo[d]imidazole-5,6-dicarboxylate