C₃₄H₄₁N₅O₆Si

Base Information

Chemical Name:C₃₄H₄₁N₅O₆Si
CAS No.:1295471-35-0
Molecular Formula:C₃₄H₄₁N₅O₆Si
Molecular Weight:643.815
Hs Code.:

C<sub>34</sub>H<sub>41</sub>N<sub>5</sub>O<sub>6</sub>Si

Synonyms:C₃₄H₄₁N₅O₆Si

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Chemical Property of C₃₄H₄₁N₅O₆Si

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Technology Process of C₃₄H₄₁N₅O₆Si

There total 10 articles about C₃₄H₄₁N₅O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₅H₄₅N₅O₇Si

: 1295471-35-0
C₃₄H₄₁N₅O₆Si

Guidance literature:: With sodium periodate; In tetrahydrofuran; water; at 20 ℃; for 3h;
DOI:10.1002/anie.201008079

Reference yield:

: 1295471-56-5
C₁₇H₂₀N₄O₅

: 1295471-35-0
C₃₄H₄₁N₅O₆Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: zinc trifluoromethanesulfonate; acetic acid / 48 h / 80 °C

1.2: 1 h / 0 - 20 °C

2.1: dmap; triethylamine / dichloromethane / 4 h / 0 - 20 °C

3.1: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 1 h / -78 - 0 °C / Inert atmosphere

4.1: ytterbium(III) triflate / toluene / 9 h / 20 - 80 °C

5.1: hydrogenchloride; water / tetrahydrofuran / 14 h / 0 - 20 °C

6.1: diisobutylaluminium hydride / dichloromethane; toluene / 2 h / -78 °C / Inert atmosphere

7.1: pyrographite; triethylamine / tetrahydrofuran / 0.25 h / -46 °C / Inert atmosphere

8.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; acetone / 2 h / 0 - 20 °C

9.1: sodium periodate / tetrahydrofuran; water / 3 h / 20 °C

With pyridine; hydrogenchloride; dmap; sodium periodate; osmium(VIII) oxide; trifluoromethylsulfonic anhydride; water; zinc trifluoromethanesulfonate; diisobutylaluminium hydride; pyrographite; acetic acid; 4-methylmorpholine N-oxide; triethylamine; ytterbium(III) triflate; In tetrahydrofuran; dichloromethane; water; acetone; toluene;
DOI:10.1002/anie.201008079

Reference yield:

: 1295471-20-3
C₃₃H₃₈N₄O₅Si

: 1295471-35-0
C₃₄H₄₁N₅O₆Si

Guidance literature:: Multi-step reaction with 6 steps

1: ytterbium(III) triflate / toluene / 9 h / 20 - 80 °C

2: hydrogenchloride; water / tetrahydrofuran / 14 h / 0 - 20 °C

3: diisobutylaluminium hydride / dichloromethane; toluene / 2 h / -78 °C / Inert atmosphere

4: pyrographite; triethylamine / tetrahydrofuran / 0.25 h / -46 °C / Inert atmosphere

5: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; acetone / 2 h / 0 - 20 °C

6: sodium periodate / tetrahydrofuran; water / 3 h / 20 °C

With hydrogenchloride; sodium periodate; osmium(VIII) oxide; water; diisobutylaluminium hydride; pyrographite; 4-methylmorpholine N-oxide; triethylamine; ytterbium(III) triflate; In tetrahydrofuran; dichloromethane; water; acetone; toluene;
DOI:10.1002/anie.201008079