4-acetyl-2-(4-methylphenyl)-1,1-diphenyl-1,2,5,6,7,8-hexahydropyrido[1,2-d][1,2,4,3λ4]triazaborine

Base Information

Chemical Name:4-acetyl-2-(4-methylphenyl)-1,1-diphenyl-1,2,5,6,7,8-hexahydropyrido[1,2-d][1,2,4,3λ4]triazaborine
CAS No.:1357027-14-5
Molecular Formula:C₂₇H₂₈BN₃O
Molecular Weight:421.35
Hs Code.:

Synonyms:4-acetyl-2-(4-methylphenyl)-1,1-diphenyl-1,2,5,6,7,8-hexahydropyrido[1,2-d][1,2,4,3λ4]triazaborine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-acetyl-2-(4-methylphenyl)-1,1-diphenyl-1,2,5,6,7,8-hexahydropyrido[1,2-d][1,2,4,3λ4]triazaborine

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 4-acetyl-2-(4-methylphenyl)-1,1-diphenyl-1,2,5,6,7,8-hexahydropyrido[1,2-d][1,2,4,3λ4]triazaborine

There total 3 articles about 4-acetyl-2-(4-methylphenyl)-1,1-diphenyl-1,2,5,6,7,8-hexahydropyrido[1,2-d][1,2,4,3λ4]triazaborine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 1357027-02-1
3-methyl-4-(4-methylphenyldiazenyl)-1,1-diphenyl-5,6,7,8-tetrahydropyrido[1,2-c][1,3,2λ4]oxazaborine

: 1357027-14-5
4-acetyl-2-(4-methylphenyl)-1,1-diphenyl-1,2,5,6,7,8-hexahydropyrido[1,2-d][1,2,4,3λ4]triazaborine

Guidance literature:: In dimethyl sulfoxide; for 2h; Reflux;
DOI:10.1016/j.jorganchem.2011.11.004

Reference yield:

: 5693-62-9
2,3,4,5-tetrahydro-6-methoxypyridine

: 1357027-14-5
4-acetyl-2-(4-methylphenyl)-1,1-diphenyl-1,2,5,6,7,8-hexahydropyrido[1,2-d][1,2,4,3λ4]triazaborine

Guidance literature:: Multi-step reaction with 3 steps

1: bis(acetylacetonate)nickel(II) / 24 h / 100 °C

2: dichloromethane / 24 h / 5 - 20 °C

3: dimethyl sulfoxide / 2 h / Reflux

With bis(acetylacetonate)nickel(II); In dichloromethane; dimethyl sulfoxide;
DOI:10.1016/j.jorganchem.2011.11.004

Reference yield:

: 60807-16-1
(α-hexahydropyridylidene)-propanone

: 3855-90-1
4-methylbenzenediazonium tetraphenylborate

: 1357027-14-5
4-acetyl-2-(4-methylphenyl)-1,1-diphenyl-1,2,5,6,7,8-hexahydropyrido[1,2-d][1,2,4,3λ4]triazaborine

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 24 h / 5 - 20 °C

2: dimethyl sulfoxide / 2 h / Reflux

In dichloromethane; dimethyl sulfoxide;
DOI:10.1016/j.jorganchem.2011.11.004