(3-allyloxy-5-{3-allyloxy-5-[3-allyloxy-5-(tetrahydro-pyran-2-yloxymethyl)-benzylsulfanylmethyl]-benzylsulfanylmethyl}-phenyl)-methanol

Base Information

Chemical Name:(3-allyloxy-5-{3-allyloxy-5-[3-allyloxy-5-(tetrahydro-pyran-2-yloxymethyl)-benzylsulfanylmethyl]-benzylsulfanylmethyl}-phenyl)-methanol
CAS No.:872115-36-1
Molecular Formula:C₃₈H₄₆O₆S₂
Molecular Weight:662.912
Hs Code.:

Synonyms:(3-allyloxy-5-{3-allyloxy-5-[3-allyloxy-5-(tetrahydro-pyran-2-yloxymethyl)-benzylsulfanylmethyl]-benzylsulfanylmethyl}-phenyl)-methanol

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Chemical Property of (3-allyloxy-5-{3-allyloxy-5-[3-allyloxy-5-(tetrahydro-pyran-2-yloxymethyl)-benzylsulfanylmethyl]-benzylsulfanylmethyl}-phenyl)-methanol

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Technology Process of (3-allyloxy-5-{3-allyloxy-5-[3-allyloxy-5-(tetrahydro-pyran-2-yloxymethyl)-benzylsulfanylmethyl]-benzylsulfanylmethyl}-phenyl)-methanol

There total 5 articles about (3-allyloxy-5-{3-allyloxy-5-[3-allyloxy-5-(tetrahydro-pyran-2-yloxymethyl)-benzylsulfanylmethyl]-benzylsulfanylmethyl}-phenyl)-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 110-87-2
3,4-dihydro-2H-pyran

: 872115-28-1
{3-allyloxy-5-[3-allyloxy-5-(3-allyloxy-5-hydroxymethyl-benzylsulfanylmethyl)-benzylsulfanylmethyl]-phenyl}-methanol

: 872115-36-1
(3-allyloxy-5-{3-allyloxy-5-[3-allyloxy-5-(tetrahydro-pyran-2-yloxymethyl)-benzylsulfanylmethyl]-benzylsulfanylmethyl}-phenyl)-methanol

: 872115-33-8
C₄₃H₅₄O₇S₂

Guidance literature:: With methanesulfonic acid; In tetrahydrofuran; at 20 ℃;
DOI:10.1246/bcsj.78.1773

Reference yield:

: 156204-47-6
[5-(prop-2-en-1-yloxy)benzene-1,3-diyl]dimethanol

: 872115-36-1
(3-allyloxy-5-{3-allyloxy-5-[3-allyloxy-5-(tetrahydro-pyran-2-yloxymethyl)-benzylsulfanylmethyl]-benzylsulfanylmethyl}-phenyl)-methanol

Guidance literature:: Multi-step reaction with 3 steps

1: 28 percent / phosphorus tribromide; pyridine / CH₂Cl₂ / 24 h / 20 °C

2: 2.75 g / NaOH / tetrahydrofuran; methanol; H₂O / 0 - 20 °C

3: 48 percent / methanesulfonic acid / tetrahydrofuran / 20 °C

With pyridine; sodium hydroxide; methanesulfonic acid; phosphorus tribromide; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1246/bcsj.78.1773

Reference yield:

: 872115-26-9
1-allyloxy-3,5-bis(bromomethyl)benzene

: 872115-36-1
(3-allyloxy-5-{3-allyloxy-5-[3-allyloxy-5-(tetrahydro-pyran-2-yloxymethyl)-benzylsulfanylmethyl]-benzylsulfanylmethyl}-phenyl)-methanol

Guidance literature:: Multi-step reaction with 3 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 5 h / 20 °C

2: 2.75 g / NaOH / tetrahydrofuran; methanol; H₂O / 0 - 20 °C

3: 48 percent / methanesulfonic acid / tetrahydrofuran / 20 °C

With sodium hydroxide; methanesulfonic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; methanol; water;
DOI:10.1246/bcsj.78.1773