Thioacetic acid S-(3-allyloxy-5-{3-allyloxy-5-[3-allyloxy-5-(tetrahydro-pyran-2-yloxymethyl)-benzylsulfanylmethyl]-benzylsulfanylmethyl}-benzyl) ester

Base Information

Chemical Name:Thioacetic acid S-(3-allyloxy-5-{3-allyloxy-5-[3-allyloxy-5-(tetrahydro-pyran-2-yloxymethyl)-benzylsulfanylmethyl]-benzylsulfanylmethyl}-benzyl) ester
CAS No.:872115-39-4
Molecular Formula:C₄₀H₄₈O₆S₃
Molecular Weight:721.016
Hs Code.:

Thioacetic acid S-(3-allyloxy-5-{3-allyloxy-5-[3-allyloxy-5-(tetrahydro-pyran-2-yloxymethyl)-benzylsulfanylmethyl]-benzylsulfanylmethyl}-benzyl) ester

Synonyms:Thioacetic acid S-(3-allyloxy-5-{3-allyloxy-5-[3-allyloxy-5-(tetrahydro-pyran-2-yloxymethyl)-benzylsulfanylmethyl]-benzylsulfanylmethyl}-benzyl) ester

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Chemical Property of Thioacetic acid S-(3-allyloxy-5-{3-allyloxy-5-[3-allyloxy-5-(tetrahydro-pyran-2-yloxymethyl)-benzylsulfanylmethyl]-benzylsulfanylmethyl}-benzyl) ester

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Technology Process of Thioacetic acid S-(3-allyloxy-5-{3-allyloxy-5-[3-allyloxy-5-(tetrahydro-pyran-2-yloxymethyl)-benzylsulfanylmethyl]-benzylsulfanylmethyl}-benzyl) ester

There total 6 articles about Thioacetic acid S-(3-allyloxy-5-{3-allyloxy-5-[3-allyloxy-5-(tetrahydro-pyran-2-yloxymethyl)-benzylsulfanylmethyl]-benzylsulfanylmethyl}-benzyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: methanesulfonic acid 3-allyloxy-5-{3-allyloxy-5-[3-allyloxy-5-(tetrahydro-pyran-2-yloxymethyl)-benzylsulfanylmethyl]-benzylsulfanylmethyl}-benzyl ester

: 507-09-5
tiolacetic acid

: 872115-39-4
Thioacetic acid S-(3-allyloxy-5-{3-allyloxy-5-[3-allyloxy-5-(tetrahydro-pyran-2-yloxymethyl)-benzylsulfanylmethyl]-benzylsulfanylmethyl}-benzyl) ester

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 20 ℃; for 5h;
DOI:10.1246/bcsj.78.1773

Reference yield:

: 156204-47-6
[5-(prop-2-en-1-yloxy)benzene-1,3-diyl]dimethanol

: 872115-39-4
Thioacetic acid S-(3-allyloxy-5-{3-allyloxy-5-[3-allyloxy-5-(tetrahydro-pyran-2-yloxymethyl)-benzylsulfanylmethyl]-benzylsulfanylmethyl}-benzyl) ester

Guidance literature:: Multi-step reaction with 5 steps

1: 28 percent / phosphorus tribromide; pyridine / CH₂Cl₂ / 24 h / 20 °C

2: 2.75 g / NaOH / tetrahydrofuran; methanol; H₂O / 0 - 20 °C

3: 48 percent / methanesulfonic acid / tetrahydrofuran / 20 °C

4: triethylamine / CH₂Cl₂ / 0 °C

5: 425 mg / 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 5 h / 20 °C

With pyridine; sodium hydroxide; methanesulfonic acid; phosphorus tribromide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1246/bcsj.78.1773

Reference yield:

: 872115-26-9
1-allyloxy-3,5-bis(bromomethyl)benzene

: 872115-39-4
Thioacetic acid S-(3-allyloxy-5-{3-allyloxy-5-[3-allyloxy-5-(tetrahydro-pyran-2-yloxymethyl)-benzylsulfanylmethyl]-benzylsulfanylmethyl}-benzyl) ester

Guidance literature:: Multi-step reaction with 5 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 5 h / 20 °C

2: 2.75 g / NaOH / tetrahydrofuran; methanol; H₂O / 0 - 20 °C

3: 48 percent / methanesulfonic acid / tetrahydrofuran / 20 °C

4: triethylamine / CH₂Cl₂ / 0 °C

5: 425 mg / 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 5 h / 20 °C

With sodium hydroxide; methanesulfonic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1246/bcsj.78.1773