Technology Process of C34H48O11
There total 6 articles about C34H48O11 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C66H72O15;
With
methanol; sodium methylate;
In
chloroform;
for 1h;
Inert atmosphere;
In
methanol; chloroform;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydroxide; water / tetrahydrofuran; methanol / 0.5 h
2.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve; Inert atmosphere
2.2: 16 h / 20 °C / Cooling with ice-salt bath
3.1: sodium methylate; methanol / chloroform / 1 h / 20 °C / Inert atmosphere
With
methanol; water; sodium methylate; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; chloroform;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: pyridine / chloroform / 6 h / 0 - 20 °C
2.1: hydrogen bromide; acetic acid / chloroform / 0 - 20 °C
3.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve; Inert atmosphere
3.2: 16 h / 20 °C / Cooling with ice-salt bath
4.1: sodium methylate; methanol / chloroform / 1 h / 20 °C / Inert atmosphere
With
pyridine; methanol; hydrogen bromide; sodium methylate; acetic acid;
In
dichloromethane; chloroform;