1-(2-(1,3-dioxolan-2-yl)phenyl)-1,3-dimethyl-3-(3-(3-(2-bromophenyl)-1,3-dimethyl-ureido)phenyl)urea

Base Information

Chemical Name:1-(2-(1,3-dioxolan-2-yl)phenyl)-1,3-dimethyl-3-(3-(3-(2-bromophenyl)-1,3-dimethyl-ureido)phenyl)urea
CAS No.:1114451-25-0
Molecular Formula:C₂₇H₂₉BrN₄O₄
Molecular Weight:553.456
Hs Code.:

Synonyms:1-(2-(1,3-dioxolan-2-yl)phenyl)-1,3-dimethyl-3-(3-(3-(2-bromophenyl)-1,3-dimethyl-ureido)phenyl)urea

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Chemical Property of 1-(2-(1,3-dioxolan-2-yl)phenyl)-1,3-dimethyl-3-(3-(3-(2-bromophenyl)-1,3-dimethyl-ureido)phenyl)urea

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Technology Process of 1-(2-(1,3-dioxolan-2-yl)phenyl)-1,3-dimethyl-3-(3-(3-(2-bromophenyl)-1,3-dimethyl-ureido)phenyl)urea

There total 1 articles about 1-(2-(1,3-dioxolan-2-yl)phenyl)-1,3-dimethyl-3-(3-(3-(2-bromophenyl)-1,3-dimethyl-ureido)phenyl)urea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1114451-34-1
1-(2-(1,3-dioxolan-2-yl)phenyl)-3-(3-(3-(2-bromophenyl)ureido)phenyl)urea

: 74-88-4
methyl iodide

: 1114451-25-0
1-(2-(1,3-dioxolan-2-yl)phenyl)-1,3-dimethyl-3-(3-(3-(2-bromophenyl)-1,3-dimethyl-ureido)phenyl)urea

Guidance literature:: 1-(2-(1,3-dioxolan-2-yl)phenyl)-3-(3-(3-(2-bromophenyl)ureido)phenyl)urea; With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;

methyl iodide; In N,N-dimethyl-formamide; at 20 ℃; for 21h; Inert atmosphere;
DOI:10.1039/b817527f

Reference yield: 61.0%

: 1114451-25-0
1-(2-(1,3-dioxolan-2-yl)phenyl)-1,3-dimethyl-3-(3-(3-(2-bromophenyl)-1,3-dimethyl-ureido)phenyl)urea

: 60011-16-7
(_S_S)-(+)-tert-butyl tert-butanethiosulfinate

: 1114451-36-3
1-(2-(1,3-dioxolan-2-yl)phenyl)-1,3-dimethyl-3-(3-(3-phenyl-1,3-dimethyl-ureido)phenyl)urea

: 1114451-35-2
1-(2-(1,3-dioxolan-2-yl)phenyl)-1,3-dimethyl-3-(3-(3-(2-(tert-butylsulfinyl)phenyl)-1,3-dimethyl-ureido)phenyl)urea

Guidance literature:: 1-(2-(1,3-dioxolan-2-yl)phenyl)-1,3-dimethyl-3-(3-(3-(2-bromophenyl)-1,3-dimethyl-ureido)phenyl)urea; With n-butyllithium; In tetrahydrofuran; hexane; at -90 ℃; Inert atmosphere;

(_S_S)-(+)-tert-butyl tert-butanethiosulfinate; In tetrahydrofuran; hexane; at -90 - 20 ℃; for 18h; Inert atmosphere;
DOI:10.1039/b817527f